Zeitschrift fur Anorganische und Allgemeine Chemie

, volume 623 , issue 7 , pages 1144-1150

Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane

Galina S. Zaitseva ¹

Sergei S Karlov ¹

Andrei V. Churakov ²

Judith A. Howard ²

Evgeni V Avtomonov ³

Jrg Lorberth ³

Hide authors affiliations Show authors affiliations: 3 affiliations

Moscow / Russia, Moscow State University, Chemistry Department |

Durham/England, University of Durham, Department of Chemistry |

Marburg/Lahn/Germany, Philipps-Universität Marburg, Fachbereich Chemie |

Publication type: Journal Article

Publication date: 1997-07-01

Wiley

Zeitschrift fur Anorganische und Allgemeine Chemie

scimago Q3

SJR: 0.292

CiteScore: 2.7

Impact factor: —

ISSN: 00442313, 15213749, 08631786

DOI: 10.1002/zaac.19976230723

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Inorganic Chemistry

Abstract

Syntheses of the title compounds, viz. N(CH2CH2O)3GeY (2 YFluorenyl; 4 YPhCC) by the reaction of X3GeY (1 YFluorenyl, XBr; 5 YPhCC, XCl) with N(CH2CH2OSnR3)3 (3 REt; 6 RBu) are reported including the preparation of the new compound 1. Identity and structures were established by elemental analyses, 1H and 13C NMR spectroscopy. 2 and 4 were characterized by mass spectrometry. Single crystal structures of 1, 2 and 4 were determined by X-ray diffraction methods. Darstellung, Charakterisierung und Strukturen von 1-(9-Fluorenyl)germatran and 1-(Phenylacetylenyl)germatran Uber die Synthesen der Titelverbindungen, namlich N(CH2CH2O)3GeY (2 YFluorenyl; 4 YPhCC) durch Reaktion von X3GeY (1 YFluorenyl, XBr; 5 YPhCC, XCl) mit N(CH2CH2OSnR3)3 (3 REt; 6 RBu) wird berichtet und die Darstellung der neuen Verbindung 1 wird beschrieben. Die Strukturen der Verbindungen wurden durch Elementaranalysen sowie mittels 1H and 13C NMR-Spektroskopie bestimmt, 2 und 4 massenspektrometrisch charakterisiert. 1, 2 und 4 wurden mit Rontgenbeugungsmethoden analysiert.

Found

8 citations

Churakov Andrei

PhD in Chemistry

553 publications, 7 015 citations, 13 reviews

h-index: 37

Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences

2 citations

Tyurin Daniil

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PhD in Chemistry

69 publications, 680 citations

h-index: 15

Lomonosov Moscow State University

Computational chemistry

Computational methods in chemistry

Cryogenic technology

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High-performance computing

IR spectroscopy

Interaction of X-ray and synchrotron radiation with matter

Matrix isolation

Molecular modeling

Molecular spectroscopy

Non-covalent Interactions

Non-valent interactions

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Zaitseva G. S. et al. Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane // Zeitschrift fur Anorganische und Allgemeine Chemie. 1997. Vol. 623. No. 7. pp. 1144-1150.

GOST all authors (up to 50) Copy

Zaitseva G. S., Karlov S. S., Churakov A. V., Howard J. A., Avtomonov E. V., Lorberth J. Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane // Zeitschrift fur Anorganische und Allgemeine Chemie. 1997. Vol. 623. No. 7. pp. 1144-1150.

RIS |

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TY - JOUR

DO - 10.1002/zaac.19976230723

UR - https://onlinelibrary.wiley.com/doi/10.1002/zaac.19976230723

TI - Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane

T2 - Zeitschrift fur Anorganische und Allgemeine Chemie

AU - Zaitseva, Galina S.

AU - Karlov, Sergei S

AU - Churakov, Andrei V.

AU - Howard, Judith A.

AU - Avtomonov, Evgeni V

AU - Lorberth, Jrg

PY - 1997

DA - 1997/07/01

PB - Wiley

SP - 1144-1150

IS - 7

VL - 623

SN - 0044-2313

SN - 1521-3749

SN - 0863-1786

ER -

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@article{1997_Zaitseva,

author = {Galina S. Zaitseva and Sergei S Karlov and Andrei V. Churakov and Judith A. Howard and Evgeni V Avtomonov and Jrg Lorberth},

title = {Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane},

journal = {Zeitschrift fur Anorganische und Allgemeine Chemie},

year = {1997},

volume = {623},

publisher = {Wiley},

month = {jul},

url = {https://onlinelibrary.wiley.com/doi/10.1002/zaac.19976230723},

number = {7},

pages = {1144--1150},

doi = {10.1002/zaac.19976230723}

}

MLA

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Zaitseva, Galina S., et al. “Synthesis, characterization, and structures of 1-(9-fluorenyl)-germatrane and 1-(phenylacetylenyl)germatrane.” Zeitschrift fur Anorganische und Allgemeine Chemie, vol. 623, no. 7, Jul. 1997, pp. 1144-1150. https://onlinelibrary.wiley.com/doi/10.1002/zaac.19976230723.