Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl)
Publication type: Journal Article
Publication date: 2004-10-21
scimago Q3
SJR: 0.292
CiteScore: 2.7
Impact factor: —
ISSN: 00442313, 15213749, 08631786
Inorganic Chemistry
Abstract
Supermesityl selenium diimide [Se{N(C6H2tBu3-2, 4, 6)}2; Se{N(mes*)}2] can be prepared in a good yield from the reaction of SeCl4 and (mes*)NHLi. The molecule adopts an unprecedented anti, anti-conformation, as deduced by DFT calculations at PBE0/TZVP level of theory and supported by 77Se NMR spectroscopy and a crystal structure determination. An analogous reaction involving (C6H2Me3-2, 4, 6)NHLi [(mes)NHLi] unexpectedly lead to the reduction of selenium and afforded the selenium diamide Se{NH(mes)}2 that was characterized by X-ray crystallography and 77Se NMR spectroscopy. The Se-N bonds of 1.847(3) and 1.852(3) A show normal single bond lengths. The
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Maaninen T. et al. Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl) // Zeitschrift fur Anorganische und Allgemeine Chemie. 2004. Vol. 630. No. 12. pp. 1947-1954.
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Maaninen T., Tuononen H. M., Kosunen K., Oilunkaniemi R., Hiitola J., Laitinen R. S., Chivers T. Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl) // Zeitschrift fur Anorganische und Allgemeine Chemie. 2004. Vol. 630. No. 12. pp. 1947-1954.
Cite this
RIS
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TY - JOUR
DO - 10.1002/zaac.200400286
UR - https://doi.org/10.1002/zaac.200400286
TI - Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl)
T2 - Zeitschrift fur Anorganische und Allgemeine Chemie
AU - Maaninen, Tiina
AU - Tuononen, Heikki M
AU - Kosunen, Katja
AU - Oilunkaniemi, Raija
AU - Hiitola, Johanna
AU - Laitinen, Risto S.
AU - Chivers, Tristram
PY - 2004
DA - 2004/10/21
PB - Wiley
SP - 1947-1954
IS - 12
VL - 630
SN - 0044-2313
SN - 1521-3749
SN - 0863-1786
ER -
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BibTex (up to 50 authors)
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@article{2004_Maaninen,
author = {Tiina Maaninen and Heikki M Tuononen and Katja Kosunen and Raija Oilunkaniemi and Johanna Hiitola and Risto S. Laitinen and Tristram Chivers},
title = {Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl)},
journal = {Zeitschrift fur Anorganische und Allgemeine Chemie},
year = {2004},
volume = {630},
publisher = {Wiley},
month = {oct},
url = {https://doi.org/10.1002/zaac.200400286},
number = {12},
pages = {1947--1954},
doi = {10.1002/zaac.200400286}
}
Cite this
MLA
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Maaninen, Tiina, et al. “Formation, Structural Characterization, and Calculated NMR Chemical Shifts of Selenium-Nitrogen Compounds from SeCl4 and ArNHLi (Ar = supermesityl, mesityl).” Zeitschrift fur Anorganische und Allgemeine Chemie, vol. 630, no. 12, Oct. 2004, pp. 1947-1954. https://doi.org/10.1002/zaac.200400286.