Zeitschrift fur Anorganische und Allgemeine Chemie

, том 637 , издание 12 , страницы 1761-1768

About the Reaction of BeCl2 with the Carbodiphosphorane Addition Compound O2C←C(PPh3)2 and its Hydrolysis Product Ph3PCHP(O)Ph2

Тип публикации: Journal Article

Дата публикации: 2011-09-05

Wiley

Zeitschrift fur Anorganische und Allgemeine Chemie

scimago Q3

БС3

SJR: 0.292

CiteScore: 2.7

Impact factor: 1.1

ISSN: 00442313, 15213749, 08631786

DOI: 10.1002/zaac.201100293

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Inorganic Chemistry

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Abstract. Reaction of BeCl2 and (PPh4)[Be2Cl6] with Ph3PCHP(O)Ph2 (2) and of BeCl2 with O2C←C(PPh3)2 (3) were studied under various conditions. Whereas the addition compound of 2 with BeCl2 could only traced by 31P NMR spectroscopy the molecular structure of the O-addition compound [Ph3PCH2P(OBeCl3)Ph2]·0.75CH2Cl2 (5) from 2 and (PPh4)[Be2Cl6] could be performed. From 3 and BeCl2 in dichloromethane crystals of (H2C{PPh3}2)[BeCl4] (6) and (H2C{PPh3}2)Cl2·CH2Cl2 (7) separated. The cluster [Be6(OH)6Cl5(O2C2{PPh3}2)3]Cl(8) formed upon unintentionally admitting some humidity to the initial reaction mixture. In 8 each of the bidentate ligands 3 bridges two different beryllium atoms via the oxygen atoms. All compounds are characterized by X-ray diffraction analyses.

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European Journal of Inorganic Chemistry	European Journal of Inorganic Chemistry, 3, 16.67% European Journal of Inorganic Chemistry 3 публикации, 16.67%
Zeitschrift fur Anorganische und Allgemeine Chemie	Zeitschrift fur Anorganische und Allgemeine Chemie, 2, 11.11% Zeitschrift fur Anorganische und Allgemeine Chemie 2 публикации, 11.11%
Dalton Transactions	Dalton Transactions, 2, 11.11% Dalton Transactions 2 публикации, 11.11%
Coordination Chemistry Reviews	Coordination Chemistry Reviews, 1, 5.56% Coordination Chemistry Reviews 1 публикация, 5.56%
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ACS Catalysis	ACS Catalysis, 1, 5.56% ACS Catalysis 1 публикация, 5.56%
Inorganic Chemistry	Inorganic Chemistry, 1, 5.56% Inorganic Chemistry 1 публикация, 5.56%
Annual Reports Section A (Inorganic Chemistry)	Annual Reports Section A (Inorganic Chemistry), 1, 5.56% Annual Reports Section A (Inorganic Chemistry) 1 публикация, 5.56%
Chemical Science	Chemical Science, 1, 5.56% Chemical Science 1 публикация, 5.56%
Acta Crystallographica Section E: Crystallographic Communications	Acta Crystallographica Section E: Crystallographic Communications, 1, 5.56% Acta Crystallographica Section E: Crystallographic Communications 1 публикация, 5.56%
Chemical Record	Chemical Record, 1, 5.56% Chemical Record 1 публикация, 5.56%
X-ray Structure Analysis Online	X-ray Structure Analysis Online, 1, 5.56% X-ray Structure Analysis Online 1 публикация, 5.56%
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International Union of Crystallography (IUCr)	International Union of Crystallography (IUCr), 1, 5.56% International Union of Crystallography (IUCr) 1 публикация, 5.56%
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Petz W., Dehnicke K., Neumüller B. About the Reaction of BeCl2 with the Carbodiphosphorane Addition Compound O2C←C(PPh3)2 and its Hydrolysis Product Ph3PCHP(O)Ph2 // Zeitschrift fur Anorganische und Allgemeine Chemie. 2011. Vol. 637. No. 12. pp. 1761-1768.

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TY - JOUR

DO - 10.1002/zaac.201100293

UR - https://doi.org/10.1002/zaac.201100293

TI - About the Reaction of BeCl2 with the Carbodiphosphorane Addition Compound O2C←C(PPh3)2 and its Hydrolysis Product Ph3PCHP(O)Ph2

T2 - Zeitschrift fur Anorganische und Allgemeine Chemie

AU - Petz, Wolfgang

AU - Dehnicke, Kurt

AU - Neumüller, Bernhard

PY - 2011

DA - 2011/09/05

PB - Wiley

SP - 1761-1768

IS - 12

VL - 637

SN - 0044-2313

SN - 1521-3749

SN - 0863-1786

ER -

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@article{2011_Petz,

author = {Wolfgang Petz and Kurt Dehnicke and Bernhard Neumüller},

title = {About the Reaction of BeCl2 with the Carbodiphosphorane Addition Compound O2C←C(PPh3)2 and its Hydrolysis Product Ph3PCHP(O)Ph2},

journal = {Zeitschrift fur Anorganische und Allgemeine Chemie},

year = {2011},

volume = {637},

publisher = {Wiley},

month = {sep},

url = {https://doi.org/10.1002/zaac.201100293},

number = {12},

pages = {1761--1768},

doi = {10.1002/zaac.201100293}

}

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Petz, Wolfgang, et al. “About the Reaction of BeCl2 with the Carbodiphosphorane Addition Compound O2C←C(PPh3)2 and its Hydrolysis Product Ph3PCHP(O)Ph2.” Zeitschrift fur Anorganische und Allgemeine Chemie, vol. 637, no. 12, Sep. 2011, pp. 1761-1768. https://doi.org/10.1002/zaac.201100293.

Издатель

Wiley

Журнал

Zeitschrift fur Anorganische und Allgemeine Chemie

scimago Q3

БС3

SJR

0.292

CiteScore

2.7

Impact factor

1.1

ISSN

00442313 (Print)

15213749 (Electronic)

08631786 (Print)