Synthesis and NMR spectra of [15N]indole
Тип публикации: Journal Article
Дата публикации: 2023-09-01
SCImago Q3
WOS Q3
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SJR: 0.281
CiteScore: 2.7
Impact factor: 1.2
ISSN: 00093122, 15738353
Organic Chemistry
Краткое описание
A method was developed for the synthesis of selectively labeled [15N]indole, allowing to obtain the target product with high chemical and isotopic purity. One-dimensional and two-dimensional 1H, 13C, and 15N NMR spectra were examined. The chemical shifts of 1H, 13C, and 15N nuclei were determined, as well as the spin-spin coupling constants of 15N nucleus and the isotopic chemical shifts of 13C nuclei for [15N]indole in CD3CN solution, caused by the replacement of 14N nucleus with a 15N nucleus. It was demonstrated that isotopic shifts of this type can provide important structural information. The NMR data set obtained in the current work can serve as an important reference point for establishing the structures of new aromatic heterocycles.
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Chemistry of Heterocyclic Compounds
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Shestakova A. K., Stanishevskiy V. V., Chertkov V. A. Synthesis and NMR spectra of [15N]indole // Chemistry of Heterocyclic Compounds. 2023. Vol. 59. No. 9-10. pp. 657-665.
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Shestakova A. K., Stanishevskiy V. V., Chertkov V. A. Synthesis and NMR spectra of [15N]indole // Chemistry of Heterocyclic Compounds. 2023. Vol. 59. No. 9-10. pp. 657-665.
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TY - JOUR
DO - 10.1007/s10593-023-03251-6
UR - https://doi.org/10.1007/s10593-023-03251-6
TI - Synthesis and NMR spectra of [15N]indole
T2 - Chemistry of Heterocyclic Compounds
AU - Shestakova, Alla K.
AU - Stanishevskiy, Vladislav V
AU - Chertkov, Vyacheslav A
PY - 2023
DA - 2023/09/01
PB - Springer Nature
SP - 657-665
IS - 9-10
VL - 59
SN - 0009-3122
SN - 1573-8353
ER -
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@article{2023_Shestakova,
author = {Alla K. Shestakova and Vladislav V Stanishevskiy and Vyacheslav A Chertkov},
title = {Synthesis and NMR spectra of [15N]indole},
journal = {Chemistry of Heterocyclic Compounds},
year = {2023},
volume = {59},
publisher = {Springer Nature},
month = {sep},
url = {https://doi.org/10.1007/s10593-023-03251-6},
number = {9-10},
pages = {657--665},
doi = {10.1007/s10593-023-03251-6}
}
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Shestakova, Alla K., et al. “Synthesis and NMR spectra of [15N]indole.” Chemistry of Heterocyclic Compounds, vol. 59, no. 9-10, Sep. 2023, pp. 657-665. https://doi.org/10.1007/s10593-023-03251-6.
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