Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines
Publication type: Journal Article
Publication date: 2014-08-13
scimago Q2
wos Q2
SJR: 0.528
CiteScore: 5.7
Impact factor: 3.5
ISSN: 09226168, 15685675
General Chemistry
Abstract
Silica gel has been found to be an efficient and reusable medium for the synthesis of diastereospecific functionalized piperidines in good to high yields by a one-pot three-component condensation of aldehyde, amine and β-ketoester under solvent-free conditions at room temperature. Using this environmentally benign, non-inflammable and non-toxic reaction medium, the non-chromatographic purification, reusability of the silica gel, and operational simplicity are the notable advantages of the present method. The procedure is applicable for large-scale synthesis of piperidines derivatives and represents a green synthetic protocol.
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Das S. et al. Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines // Research on Chemical Intermediates. 2014. Vol. 41. No. 9. pp. 6749-6763.
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Das S., Bagdi A. K., Santra S., Majee A., Hajra A. Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines // Research on Chemical Intermediates. 2014. Vol. 41. No. 9. pp. 6749-6763.
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TY - JOUR
DO - 10.1007/s11164-014-1774-7
UR - https://doi.org/10.1007/s11164-014-1774-7
TI - Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines
T2 - Research on Chemical Intermediates
AU - Das, Sudarshan
AU - Bagdi, Avik Kumar
AU - Santra, Sougata
AU - Majee, Adinath
AU - Hajra, Alakananda
PY - 2014
DA - 2014/08/13
PB - Springer Nature
SP - 6749-6763
IS - 9
VL - 41
SN - 0922-6168
SN - 1568-5675
ER -
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@article{2014_Das,
author = {Sudarshan Das and Avik Kumar Bagdi and Sougata Santra and Adinath Majee and Alakananda Hajra},
title = {Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines},
journal = {Research on Chemical Intermediates},
year = {2014},
volume = {41},
publisher = {Springer Nature},
month = {aug},
url = {https://doi.org/10.1007/s11164-014-1774-7},
number = {9},
pages = {6749--6763},
doi = {10.1007/s11164-014-1774-7}
}
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MLA
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Das, Sudarshan, et al. “Solvent-free silica-promoted multicomponent condensation: synthesis of highly functionalized piperidines.” Research on Chemical Intermediates, vol. 41, no. 9, Aug. 2014, pp. 6749-6763. https://doi.org/10.1007/s11164-014-1774-7.