Springer Nature
Russian Chemical Bulletin
,  volume 59 ,  issue 11 ,  pages 2081-2085

Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps

Publication type: Journal Article
Publication date: 2010-11-01
Springer Nature
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The reactions of 5,5-dimethyl-3-oxo-1-pyrroline 1-oxide (3-oxo-DMPO, 1) with NH2OH and N2H4 afforded oxime (2a) and hydrazone (2b), respectively. The reaction products were studied as spin traps for the short-lived radicals HO·, Ph·, PhCO2 ·, NC(Me2)C·, and NC(Me2)CO·. The nitroxides generated in the reactions of the above-mentioned short-lived radicals with nitrones 1 and 2a,b were characterized by ESR spectroscopy. Of these nitrones, oxime 2a is the most effective radical trap.
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Golubev V. A., Shilov G. V., Sen V. D. Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps // Russian Chemical Bulletin. 2010. Vol. 59. No. 11. pp. 2081-2085.
GOST all authors (up to 50) Copy
Golubev V. A., Shilov G. V., Sen V. D. Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps // Russian Chemical Bulletin. 2010. Vol. 59. No. 11. pp. 2081-2085.
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RIS Copy
TY - JOUR
DO - 10.1007/s11172-010-0358-y
UR - https://doi.org/10.1007/s11172-010-0358-y
TI - Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps
T2 - Russian Chemical Bulletin
AU - Golubev, V. A.
AU - Shilov, G V
AU - Sen, V D
PY - 2010
DA - 2010/11/01
PB - Springer Nature
SP - 2081-2085
IS - 11
VL - 59
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2010_Golubev,
author = {V. A. Golubev and G V Shilov and V D Sen},
title = {Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps},
journal = {Russian Chemical Bulletin},
year = {2010},
volume = {59},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11172-010-0358-y},
number = {11},
pages = {2081--2085},
doi = {10.1007/s11172-010-0358-y}
}
MLA
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MLA Copy
Golubev, V. A., et al. “Synthesis of new functionalized 5,5-dimethyl-1-pyrroline 1-oxides and their investigation as spin traps.” Russian Chemical Bulletin, vol. 59, no. 11, Nov. 2010, pp. 2081-2085. https://doi.org/10.1007/s11172-010-0358-y.