Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide
Publication type: Journal Article
Publication date: 2023-10-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide from the corresponding methyl ester is described. The key step is the oxidation of (±)-(1S*,5R*)-4-oxo-5-phenylthiomethylcyclopent-2-en-1-ylacetic acid ethanolamide with gem-bis(hydroperoxy)cyclohexane.
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Makaev Z. R. et al. Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide // Russian Chemical Bulletin. 2023. Vol. 72. No. 10. pp. 2425-2429.
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Makaev Z. R., Vostrikov N. S., Gimazetdinov A. M., Selezneva N. K., Miftakhov M. S. Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide // Russian Chemical Bulletin. 2023. Vol. 72. No. 10. pp. 2425-2429.
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TY - JOUR
DO - 10.1007/s11172-023-4043-3
UR - https://doi.org/10.1007/s11172-023-4043-3
TI - Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide
T2 - Russian Chemical Bulletin
AU - Makaev, Z R
AU - Vostrikov, N S
AU - Gimazetdinov, A M
AU - Selezneva, N K
AU - Miftakhov, M S
PY - 2023
DA - 2023/10/01
PB - Springer Nature
SP - 2425-2429
IS - 10
VL - 72
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2023_Makaev,
author = {Z R Makaev and N S Vostrikov and A M Gimazetdinov and N K Selezneva and M S Miftakhov},
title = {Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide},
journal = {Russian Chemical Bulletin},
year = {2023},
volume = {72},
publisher = {Springer Nature},
month = {oct},
url = {https://doi.org/10.1007/s11172-023-4043-3},
number = {10},
pages = {2425--2429},
doi = {10.1007/s11172-023-4043-3}
}
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MLA
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Makaev, Z. R., et al. “Synthesis of (±)-5-methylidene-4-oxocyclopent-2-en-1-ylacetic acid ethanolamide.” Russian Chemical Bulletin, vol. 72, no. 10, Oct. 2023, pp. 2425-2429. https://doi.org/10.1007/s11172-023-4043-3.