Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO
Publication type: Journal Article
Publication date: 2024-07-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
Abstract
2-Azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde was synthesized by the Vilsmeier–Haack reaction. In DMSO, it transforms into 7-oxo-5-phenyl-4,7-dihydrotetrazolo[1,5-a]pyrimidine-6-carbaldehyde and then undergoes isomerization recyclization into 6-benzoyltetrazolo[1,5-a]pyrimidin-7(4H)-one. The structures of the obtained compounds were determined by NMR spectroscopy and X-ray diffraction.
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Russian Chemical Bulletin
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Springer Nature
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Aleksandrova N. V. et al. Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO // Russian Chemical Bulletin. 2024. Vol. 73. No. 7. pp. 2014-2022.
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Aleksandrova N. V., Nikolaenkova E. B., Gatilov Y., Mamatyuk V., Krivopalov V. P. Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO // Russian Chemical Bulletin. 2024. Vol. 73. No. 7. pp. 2014-2022.
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TY - JOUR
DO - 10.1007/s11172-024-4321-8
UR - https://link.springer.com/10.1007/s11172-024-4321-8
TI - Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO
T2 - Russian Chemical Bulletin
AU - Aleksandrova, N. V.
AU - Nikolaenkova, E B
AU - Gatilov, Yu.V
AU - Mamatyuk, V.I
AU - Krivopalov, V P
PY - 2024
DA - 2024/07/01
PB - Springer Nature
SP - 2014-2022
IS - 7
VL - 73
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2024_Aleksandrova,
author = {N. V. Aleksandrova and E B Nikolaenkova and Yu.V Gatilov and V.I Mamatyuk and V P Krivopalov},
title = {Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO},
journal = {Russian Chemical Bulletin},
year = {2024},
volume = {73},
publisher = {Springer Nature},
month = {jul},
url = {https://link.springer.com/10.1007/s11172-024-4321-8},
number = {7},
pages = {2014--2022},
doi = {10.1007/s11172-024-4321-8}
}
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MLA
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Aleksandrova, N. V., et al. “Synthesis of 2-azido-4-chloro-6-phenylpyrimidine-5-carbaldehyde and its transformations in DMSO.” Russian Chemical Bulletin, vol. 73, no. 7, Jul. 2024, pp. 2014-2022. https://link.springer.com/10.1007/s11172-024-4321-8.