Springer Nature
Russian Chemical Bulletin
,  volume 44 ,  issue 1 ,  pages 116-123

Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle

Publication type: Journal Article
Publication date: 1995-01-01
Springer Nature
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
A method for the synthesis of 4′-bromobenzodithia-15(18)-crown-5(6) and 4′-bromobenzodiaza-15 (18)-crown-5(6) by condensation of 3,4-di(2′-haloethoxy)bromobenzene with polyoxaalkanes containing terminal SH or NHMe groups was suggested. The method for the synthesis of formyl derivatives of benzocrowns containing N, S, and O heteroatoms in the macrocycle based on the metallation of appropriate bromo derivatives with BunLi followed by treatment of the resulting organolithium intermediates with DMF was developed. Oximes and semicarbazones of benzaldehydes containing a crown ether fragment were obtained, and their transformation into the original aldehydes by treatment with KNO2 in an acid medium was studied.
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GOST Copy
Gromov S. P. et al. Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle // Russian Chemical Bulletin. 1995. Vol. 44. No. 1. pp. 116-123.
GOST all authors (up to 50) Copy
Gromov S. P., Fedorova O., Vedernikov A., Samoshin V. V., Zefirov N. S., Alfimov M. Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle // Russian Chemical Bulletin. 1995. Vol. 44. No. 1. pp. 116-123.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1007/BF00696971
UR - http://link.springer.com/10.1007/BF00696971
TI - Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle
T2 - Russian Chemical Bulletin
AU - Gromov, S P
AU - Fedorova, O.A.
AU - Vedernikov, A.I.
AU - Samoshin, V V
AU - Zefirov, N. S.
AU - Alfimov, M.V.
PY - 1995
DA - 1995/01/01
PB - Springer Nature
SP - 116-123
IS - 1
VL - 44
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{1995_Gromov,
author = {S P Gromov and O.A. Fedorova and A.I. Vedernikov and V V Samoshin and N. S. Zefirov and M.V. Alfimov},
title = {Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle},
journal = {Russian Chemical Bulletin},
year = {1995},
volume = {44},
publisher = {Springer Nature},
month = {jan},
url = {http://link.springer.com/10.1007/BF00696971},
number = {1},
pages = {116--123},
doi = {10.1007/BF00696971}
}
MLA
Cite this
MLA Copy
Gromov, S. P., et al. “Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle.” Russian Chemical Bulletin, vol. 44, no. 1, Jan. 1995, pp. 116-123. http://link.springer.com/10.1007/BF00696971.
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