Russian Chemical Bulletin

, том 44 , издание 1 , страницы 116-123

Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle

Тип публикации: Journal Article

Дата публикации: 1995-01-01

Springer Nature

Russian Chemical Bulletin

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CiteScore: 2.8

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ISSN: 10665285, 15739171

DOI: 10.1007/BF00696971

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General Chemistry

Краткое описание

A method for the synthesis of 4′-bromobenzodithia-15(18)-crown-5(6) and 4′-bromobenzodiaza-15 (18)-crown-5(6) by condensation of 3,4-di(2′-haloethoxy)bromobenzene with polyoxaalkanes containing terminal SH or NHMe groups was suggested. The method for the synthesis of formyl derivatives of benzocrowns containing N, S, and O heteroatoms in the macrocycle based on the metallation of appropriate bromo derivatives with BunLi followed by treatment of the resulting organolithium intermediates with DMF was developed. Oximes and semicarbazones of benzaldehydes containing a crown ether fragment were obtained, and their transformation into the original aldehydes by treatment with KNO2 in an acid medium was studied.

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Вацадзе Сергей

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Институт органической химии им. Н.Д. Зелинского РАН

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Институт органической химии им. Н.Д. Зелинского РАН

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Институт общей и неорганической химии им. Н.С. Курнакова РАН

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Russian Chemical Bulletin	Russian Chemical Bulletin, 2, 25% Russian Chemical Bulletin 2 публикации, 25%
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Chemistry of Heterocyclic Compounds	Chemistry of Heterocyclic Compounds, 1, 12.5% Chemistry of Heterocyclic Compounds 1 публикация, 12.5%
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Gromov S. P. et al. Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle // Russian Chemical Bulletin. 1995. Vol. 44. No. 1. pp. 116-123.

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Gromov S. P., Fedorova O., Vedernikov A., Samoshin V. V., Zefirov N. S., Alfimov M. Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle // Russian Chemical Bulletin. 1995. Vol. 44. No. 1. pp. 116-123.

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TY - JOUR

DO - 10.1007/BF00696971

UR - http://link.springer.com/10.1007/BF00696971

TI - Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle

T2 - Russian Chemical Bulletin

AU - Gromov, S P

AU - Fedorova, O.A.

AU - Vedernikov, A.I.

AU - Samoshin, V V

AU - Zefirov, N. S.

AU - Alfimov, M.V.

PY - 1995

DA - 1995/01/01

PB - Springer Nature

SP - 116-123

IS - 1

VL - 44

SN - 1066-5285

SN - 1573-9171

ER -

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@article{1995_Gromov,

author = {S P Gromov and O.A. Fedorova and A.I. Vedernikov and V V Samoshin and N. S. Zefirov and M.V. Alfimov},

title = {Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle},

journal = {Russian Chemical Bulletin},

year = {1995},

volume = {44},

publisher = {Springer Nature},

month = {jan},

url = {http://link.springer.com/10.1007/BF00696971},

number = {1},

pages = {116--123},

doi = {10.1007/BF00696971}

}

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Gromov, S. P., et al. “Synthesis of formyl derivatives of benzocrown ethers containing N, S, and O heteroatoms in the macrocycle.” Russian Chemical Bulletin, vol. 44, no. 1, Jan. 1995, pp. 116-123. http://link.springer.com/10.1007/BF00696971.