Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5 (CH3 ) 4 (CH2 CH2 OCH3 )]ZrCl3
Publication type: Journal Article
Publication date: 1996-07-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Several novel zirconium(iv) complexes with the chelating oxygen-containing cyclopentadienyl ligand, tetramethyl(2-methoxyethyl)cyclopentadiene, have been synthesized. [η5:η1-Tetra-methyl(2-methyl)cyclopentadienyl]trichlorozirconium (2), bis[η5-tetramethyl(2-methoxyethyl)cyclopentadienyl]dichlorozirconium (3), [η5-pentamethylcyclopentadienyl][η5-tetra-methyl(2-methoxyethyl)cyclopentadienyl]dichlorozirconium (4), and [η5-tetra-methyl(2-methylthioethyl)cyclopentadienyl][η5-tetramethyl(2-methoxyethyl)-cyclopentadienyl]dichlorozirconium (5) have been prepared from the corresponding lithium cyclopentadienide (l). The crystal structure of cyclopentadienyl complex2 has been established by X-ray analysis. The coordination O→Zr bond in compound2 exists both in the crystalline state and in solutions. No coordination of this type was observed in complexes3–5. Synthesized complexes2–5 are discussed in comparison with their sulfur-containing analogs.
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Krutko D. P. et al. Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5(CH3) 4(CH2CH2OCH3)]ZrCl3 // Russian Chemical Bulletin. 1996. Vol. 45. No. 7. pp. 1740-1744.
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Krutko D. P., Borzov M. V., Petrosyan V. S., Kuz'mina L. G., Churakov A. Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5(CH3) 4(CH2CH2OCH3)]ZrCl3 // Russian Chemical Bulletin. 1996. Vol. 45. No. 7. pp. 1740-1744.
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TY - JOUR
DO - 10.1007/BF01431817
UR - http://link.springer.com/10.1007/BF01431817
TI - Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5(CH3) 4(CH2CH2OCH3)]ZrCl3
T2 - Russian Chemical Bulletin
AU - Krutko, D P
AU - Borzov, M V
AU - Petrosyan, V. S.
AU - Kuz'mina, L. G.
AU - Churakov, A.V.
PY - 1996
DA - 1996/07/01
PB - Springer Nature
SP - 1740-1744
IS - 7
VL - 45
SN - 1066-5285
SN - 1573-9171
ER -
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@article{1996_Krutko,
author = {D P Krutko and M V Borzov and V. S. Petrosyan and L. G. Kuz'mina and A.V. Churakov},
title = {Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5(CH3) 4(CH2CH2OCH3)]ZrCl3},
journal = {Russian Chemical Bulletin},
year = {1996},
volume = {45},
publisher = {Springer Nature},
month = {jul},
url = {http://link.springer.com/10.1007/BF01431817},
number = {7},
pages = {1740--1744},
doi = {10.1007/BF01431817}
}
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MLA
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Krutko, D. P., et al. “Tetramethyl(2-methoxyethyl)cyclopentadienyl complexes of zirconium(IV). Crystal structure of [η5:η1-C5(CH3) 4(CH2CH2OCH3)]ZrCl3.” Russian Chemical Bulletin, vol. 45, no. 7, Jul. 1996, pp. 1740-1744. http://link.springer.com/10.1007/BF01431817.