Russian Chemical Bulletin

, том 49 , издание 11 , страницы 1853-1858

Template effect in the synthesis of formyl derivatives of benzothiacrown compounds

Тип публикации: Journal Article

Дата публикации: 2000-11-01

Springer Nature

Russian Chemical Bulletin

scimago Q3

БС2

SJR: 0.305

CiteScore: 2.8

Impact factor: —

ISSN: 10665285, 15739171

DOI: 10.1007/BF02494923

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General Chemistry

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The condensation of 3,4-bis(2-haloethoxy)benzaldehydes with acyclic α,ω-alkanedithiols in the presence of alkali metal carbonates in dry ethanol, DMF, MeCN and their mixtures with water gives formyl derivatives of benzothiacrown compounds in high yields. The best results are attained when the radius of the hydrated metal cation fits to the crown ether cavity. In the case of Cs+, high yields were observed for crown ethers of any size and composition; this can be explained by a specific template effect of this cation. The influence of the nature of the leaving group in 3,4-bis(2-haloethoxy)benzaldehydes was established for reactions with dithiols containing no ether oxygen atoms.

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Russian Chemical Bulletin	Russian Chemical Bulletin, 3, 33.33% Russian Chemical Bulletin 3 публикации, 33.33%
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Fedorova O. et al. Template effect in the synthesis of formyl derivatives of benzothiacrown compounds // Russian Chemical Bulletin. 2000. Vol. 49. No. 11. pp. 1853-1858.

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Fedorova O., Vedernikov A., Yescheulova O., Tsapenko P. V., Pershina Yu. V., Gromov S. P. Template effect in the synthesis of formyl derivatives of benzothiacrown compounds // Russian Chemical Bulletin. 2000. Vol. 49. No. 11. pp. 1853-1858.

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TY - JOUR

DO - 10.1007/BF02494923

UR - http://link.springer.com/10.1007/BF02494923

TI - Template effect in the synthesis of formyl derivatives of benzothiacrown compounds

T2 - Russian Chemical Bulletin

AU - Fedorova, O.A.

AU - Vedernikov, A.I.

AU - Yescheulova, O.V

AU - Tsapenko, P V

AU - Pershina, Yu V

AU - Gromov, S P

PY - 2000

DA - 2000/11/01

PB - Springer Nature

SP - 1853-1858

IS - 11

VL - 49

SN - 1066-5285

SN - 1573-9171

ER -

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@article{2000_Fedorova,

author = {O.A. Fedorova and A.I. Vedernikov and O.V Yescheulova and P V Tsapenko and Yu V Pershina and S P Gromov},

title = {Template effect in the synthesis of formyl derivatives of benzothiacrown compounds},

journal = {Russian Chemical Bulletin},

year = {2000},

volume = {49},

publisher = {Springer Nature},

month = {nov},

url = {http://link.springer.com/10.1007/BF02494923},

number = {11},

pages = {1853--1858},

doi = {10.1007/BF02494923}

}

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Fedorova, O.A., et al. “Template effect in the synthesis of formyl derivatives of benzothiacrown compounds.” Russian Chemical Bulletin, vol. 49, no. 11, Nov. 2000, pp. 1853-1858. http://link.springer.com/10.1007/BF02494923.