13C NMR spectra and electronic structure of alkenylalanes
R R Muslukhov
1
,
L M Khalilov
2
,
I R Ramazanov
2
,
A Z Sharipova
2
,
A G Ibragimov
2
,
U M Dzhemilev
2
Publication type: Journal Article
Publication date: 1997-12-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The parameters of13C NMR spectra of linear and cyclic alkenylalanes synthesized from mono- and disubstituted acetylene and the simplest alkylalanes have been obtained. A strong paramagnetic effect of the aluminum atom on shielding of α- and β-carbon atoms at the double bond has been observed for the dimeric form of organoaluminum compounds (OAC) in inert solvents, unlike that for the monomeric form solvated in electron-donor solvents (Et2O, THF, and Et3N). The results were interpreted in terms of the model of the electron density redistribution on going from the dimeric structure of OAC to the monomeric one. The PM3 method describes most adequately (as compared to MNDO and AM1) the equilibrium geometry of cyclic dimers of OAC.
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Total citations:
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Citations from 2024:
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GOST
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Muslukhov R. R. et al. 13C NMR spectra and electronic structure of alkenylalanes // Russian Chemical Bulletin. 1997. Vol. 46. No. 12. pp. 2082-2085.
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Muslukhov R. R., Khalilov L. M., Ramazanov I. R., Sharipova A. Z., Ibragimov A. G., Dzhemilev U. M. 13C NMR spectra and electronic structure of alkenylalanes // Russian Chemical Bulletin. 1997. Vol. 46. No. 12. pp. 2082-2085.
Cite this
RIS
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TY - JOUR
DO - 10.1007/bf02495255
UR - https://doi.org/10.1007/bf02495255
TI - 13C NMR spectra and electronic structure of alkenylalanes
T2 - Russian Chemical Bulletin
AU - Muslukhov, R R
AU - Khalilov, L M
AU - Ramazanov, I R
AU - Sharipova, A Z
AU - Ibragimov, A G
AU - Dzhemilev, U M
PY - 1997
DA - 1997/12/01
PB - Springer Nature
SP - 2082-2085
IS - 12
VL - 46
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{1997_Muslukhov,
author = {R R Muslukhov and L M Khalilov and I R Ramazanov and A Z Sharipova and A G Ibragimov and U M Dzhemilev},
title = {13C NMR spectra and electronic structure of alkenylalanes},
journal = {Russian Chemical Bulletin},
year = {1997},
volume = {46},
publisher = {Springer Nature},
month = {dec},
url = {https://doi.org/10.1007/bf02495255},
number = {12},
pages = {2082--2085},
doi = {10.1007/bf02495255}
}
Cite this
MLA
Copy
Muslukhov, R. R., et al. “13C NMR spectra and electronic structure of alkenylalanes.” Russian Chemical Bulletin, vol. 46, no. 12, Dec. 1997, pp. 2082-2085. https://doi.org/10.1007/bf02495255.