Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system
Publication type: Journal Article
Publication date: 1994-01-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
2-Nitro-1,3-dicarbonyl and α-nitromonocarbonyl compounds were synthesized in the yields varying from moderate (30 %) to nearly quantitative by the nitration of β-dicarbonyl compounds in a two-phase system: sulfuric/nitric acid mixture-chloroform at - 10÷10 °C. The use of phase transfer conditions made it possible to avoid the formation of furoxans as by-products and to simplify the isolation of products. This method is quite common for preparing various α-functional nitro compounds including those containing a CF3-group. Key words: nitration, α-functional nitro compounds.
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GOST
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Kislyi V. P. et al. Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system // Russian Chemical Bulletin. 1994. Vol. 43. No. 1. pp. 70-74.
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Kislyi V. P., Laikhter A. L., Ugrak B. I., Semenov V. V. Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system // Russian Chemical Bulletin. 1994. Vol. 43. No. 1. pp. 70-74.
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RIS
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TY - JOUR
DO - 10.1007/bf00699138
UR - https://doi.org/10.1007/bf00699138
TI - Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system
T2 - Russian Chemical Bulletin
AU - Kislyi, V P
AU - Laikhter, A L
AU - Ugrak, B I
AU - Semenov, V. V.
PY - 1994
DA - 1994/01/01
PB - Springer Nature
SP - 70-74
IS - 1
VL - 43
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{1994_Kislyi,
author = {V P Kislyi and A L Laikhter and B I Ugrak and V. V. Semenov},
title = {Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system},
journal = {Russian Chemical Bulletin},
year = {1994},
volume = {43},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/bf00699138},
number = {1},
pages = {70--74},
doi = {10.1007/bf00699138}
}
Cite this
MLA
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Kislyi, V. P., et al. “Synthesis of ?-functional nitro compounds by the nitration of activated carbonyl compounds in a two-phase system.” Russian Chemical Bulletin, vol. 43, no. 1, Jan. 1994, pp. 70-74. https://doi.org/10.1007/bf00699138.