Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry
Publication type: Journal Article
Publication date: 1995-09-01
scimago Q3
wos Q4
SJR: 0.278
CiteScore: 2.7
Impact factor: 1.3
ISSN: 00095893, 16121112
Organic Chemistry
Biochemistry
Clinical Biochemistry
Analytical Chemistry
Abstract
Two-step liquid chromatographic separation (LC) has been applied to soot extract and the identification of higher fullerenes has been accomplished by LC-MS measurements using an ESI interface. The first separation step is preparative-scale LC using a 50 mm i.d. column packed with monomeric octadecylisilica (ODS) because elution is mainly controlled by relative molecular mass. 39 batches of five fractions each were collected and then as the second separation step each fraction was analysed by analytical-scale LC using a conventional column of a polymeric ODS phase which can elute fullerenes according to shape and structure. This stationary phase can also separate many isomers of higher fullerenes, consequently the existence of several higher fullerenes larger than C86 has been confirmed and their UV-Vis spectra were obtained by the photodiode array detection system coupled to the analytical LC.
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GOST
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Jinno K. et al. Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry // Chromatographia. 1995. Vol. 41. No. 5-6. pp. 353-360.
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Jinno K., Matsui H., Ohta H., Saito Y., Nakagawa K., Nagashima H., Itoh K. Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry // Chromatographia. 1995. Vol. 41. No. 5-6. pp. 353-360.
Cite this
RIS
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TY - JOUR
DO - 10.1007/bf02688051
UR - https://doi.org/10.1007/bf02688051
TI - Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry
T2 - Chromatographia
AU - Jinno, K.
AU - Matsui, H.
AU - Ohta, H.
AU - Saito, Y.
AU - Nakagawa, K.
AU - Nagashima, H.
AU - Itoh, K.
PY - 1995
DA - 1995/09/01
PB - Springer Nature
SP - 353-360
IS - 5-6
VL - 41
SN - 0009-5893
SN - 1612-1112
ER -
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BibTex (up to 50 authors)
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@article{1995_Jinno,
author = {K. Jinno and H. Matsui and H. Ohta and Y. Saito and K. Nakagawa and H. Nagashima and K. Itoh},
title = {Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry},
journal = {Chromatographia},
year = {1995},
volume = {41},
publisher = {Springer Nature},
month = {sep},
url = {https://doi.org/10.1007/bf02688051},
number = {5-6},
pages = {353--360},
doi = {10.1007/bf02688051}
}
Cite this
MLA
Copy
Jinno, K., et al. “Separation and identification of higher fullerenes in soot extract by liquid chromatography-mass spectrometry.” Chromatographia, vol. 41, no. 5-6, Sep. 1995, pp. 353-360. https://doi.org/10.1007/bf02688051.