Springer Nature
Polymer Bulletin
,  volume 65 ,  issue 9 ,  pages 905-916

Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties

Florica Adriana Nicolescu 1
, 
Valentin Victor Jerca 1
, 
Dumitru Mircea Vuluga 1
, 
Dan-Sorin Vasilescu 2
1
 
Centre for Organic Chemistry Costin D. Nenitescu, Romanian Academy, Bucharest, Romania | 
2
 
Publication type: Journal Article
Publication date: 2010-05-28
Springer Nature
scimago Q2
wos Q2
SJR: 0.658
CiteScore: 6.7
Impact factor: 4.0
ISSN: 01700839, 14362449
Materials Chemistry
General Chemistry
Condensed Matter Physics
Polymers and Plastics
Abstract
New side-chain poly(methacrylate)s with azo moieties were prepared by free radical copolymerization, starting from methyl methacrylate (MMA) and some original azo-monomers. The chromophore content was evaluated from 1H-NMR spectroscopy and elemental analyses; all structures exhibited a high content of azobenzene units. UV–Vis measurements have also supported this fact. Reactivity ratios for the methacrylate systems and their corresponding Q–e values were calculated based on several initial feed compositions (MMA and the newly synthesized azo-monomers) using an integral method with its appropriate software. The polymers were also characterized by FTIR, SEC and DSC-TGA techniques. The coloured poly(methacrylate)s exhibited glass transition temperatures between 141 and 168 °C and thermal stabilities up to 306 °C.
Found 
Found 

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GOST |
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GOST Copy
Nicolescu F. A. et al. Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties // Polymer Bulletin. 2010. Vol. 65. No. 9. pp. 905-916.
GOST all authors (up to 50) Copy
Nicolescu F. A., Jerca V. V., Vuluga D. M., Vasilescu D. Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties // Polymer Bulletin. 2010. Vol. 65. No. 9. pp. 905-916.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1007/s00289-010-0302-1
UR - https://doi.org/10.1007/s00289-010-0302-1
TI - Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties
T2 - Polymer Bulletin
AU - Nicolescu, Florica Adriana
AU - Jerca, Valentin Victor
AU - Vuluga, Dumitru Mircea
AU - Vasilescu, Dan-Sorin
PY - 2010
DA - 2010/05/28
PB - Springer Nature
SP - 905-916
IS - 9
VL - 65
SN - 0170-0839
SN - 1436-2449
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2010_Nicolescu,
author = {Florica Adriana Nicolescu and Valentin Victor Jerca and Dumitru Mircea Vuluga and Dan-Sorin Vasilescu},
title = {Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties},
journal = {Polymer Bulletin},
year = {2010},
volume = {65},
publisher = {Springer Nature},
month = {may},
url = {https://doi.org/10.1007/s00289-010-0302-1},
number = {9},
pages = {905--916},
doi = {10.1007/s00289-010-0302-1}
}
MLA
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MLA Copy
Nicolescu, Florica Adriana, et al. “Synthesis and characterization of side-chain poly(methacrylate)s bearing new azo-moieties.” Polymer Bulletin, vol. 65, no. 9, May. 2010, pp. 905-916. https://doi.org/10.1007/s00289-010-0302-1.