Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates
1
“ChemEx” Laboratory, Vladimir Dal’ East Ukrainian National University, Lugansk, Ukraine
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2
Scientific-Technological Complex “Institute of Monocrystals”, National Academy of Sciences of Ukraine, Kharkiv, Ukraine
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Publication type: Journal Article
Publication date: 2013-06-21
scimago Q4
wos Q4
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Abstract
10-Amino-7,11-dicyano-9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates have been obtained by the interaction of N-alkylpiperidin-4-ones with 2 equiv. cyanoselenoacetamide or with malononitrile and cyanoselenoacetamide. Aminomethylation of the obtained compounds proceeded under mild conditions and led to the formation of 8'-selenoxo-3',5',7',11'-tetraazaspiro[piperidine-4,13'-tri-cyclo[7.3.1.02,7]tridec[2]ene]-1',9'-dicarbonitriles. The structure of 1-methyl-5',11'-di(4-methyl-phenyl)-8'-selenoxo-3',5',7',11'-tetraazaspiro[piperidine-4,13'-tricyclo[7.3.1.02,7]tridec[2]ene]-1',9'-di-carbonitrile was determined by X-ray structural analysis.
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GOST
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Frolov K. A. et al. Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates // Chemistry of Heterocyclic Compounds. 2013. Vol. 49. No. 3. pp. 472-478.
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Frolov K. A., Dotsenko V. V., Krivokolysko S. G., Zubatyuk R. I., Shishkin O. V. Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates // Chemistry of Heterocyclic Compounds. 2013. Vol. 49. No. 3. pp. 472-478.
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RIS
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TY - JOUR
DO - 10.1007/s10593-013-1270-9
UR - https://doi.org/10.1007/s10593-013-1270-9
TI - Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates
T2 - Chemistry of Heterocyclic Compounds
AU - Frolov, K A
AU - Dotsenko, V V
AU - Krivokolysko, S G
AU - Zubatyuk, R I
AU - Shishkin, O. V.
PY - 2013
DA - 2013/06/21
PB - Springer Nature
SP - 472-478
IS - 3
VL - 49
SN - 0009-3122
SN - 1573-8353
ER -
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BibTex (up to 50 authors)
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@article{2013_Frolov,
author = {K A Frolov and V V Dotsenko and S G Krivokolysko and R I Zubatyuk and O. V. Shishkin},
title = {Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates},
journal = {Chemistry of Heterocyclic Compounds},
year = {2013},
volume = {49},
publisher = {Springer Nature},
month = {jun},
url = {https://doi.org/10.1007/s10593-013-1270-9},
number = {3},
pages = {472--478},
doi = {10.1007/s10593-013-1270-9}
}
Cite this
MLA
Copy
Frolov, K. A., et al. “Synthesis and aminomethylation of 9-aza-3-azoniaspiro[5,5]undeca-7,10-diene-8-selenolates.” Chemistry of Heterocyclic Compounds, vol. 49, no. 3, Jun. 2013, pp. 472-478. https://doi.org/10.1007/s10593-013-1270-9.
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