Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles
Anastasiya N Khrustaleva
1
,
Konstantin A Frolov
1
,
Victor V Dotsenko
1, 2
,
Inna V Aksenova
2
,
Sergey G Krivokolysko
1
Publication type: Journal Article
Publication date: 2017-08-01
scimago Q4
wos Q4
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Abstract
The aminomethylation reaction of 9-benzyl-2,4-dioxo-3,9-diazaspiro[5.5]undecane-1,5-dicarbonitrile hydrochloride in the presence of primary aliphatic amines and an excess of 37% aqueous formaldehyde led to the formation of 7-substituted 1'-benzyl-2,4-dioxo-1H,5Hspiro[3,7-diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitrile derivatives.
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Khrustaleva A. N. et al. Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles // Chemistry of Heterocyclic Compounds. 2017. Vol. 53. No. 8. pp. 887-891.
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Khrustaleva A. N., Frolov K. A., Dotsenko V. V., Aksenov N. A., Aksenova I. V., Krivokolysko S. G. Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles // Chemistry of Heterocyclic Compounds. 2017. Vol. 53. No. 8. pp. 887-891.
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TY - JOUR
DO - 10.1007/s10593-017-2140-7
UR - https://doi.org/10.1007/s10593-017-2140-7
TI - Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles
T2 - Chemistry of Heterocyclic Compounds
AU - Khrustaleva, Anastasiya N
AU - Frolov, Konstantin A
AU - Dotsenko, Victor V
AU - Aksenov, Nikolai A
AU - Aksenova, Inna V
AU - Krivokolysko, Sergey G
PY - 2017
DA - 2017/08/01
PB - Springer Nature
SP - 887-891
IS - 8
VL - 53
SN - 0009-3122
SN - 1573-8353
ER -
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BibTex (up to 50 authors)
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@article{2017_Khrustaleva,
author = {Anastasiya N Khrustaleva and Konstantin A Frolov and Victor V Dotsenko and Nikolai A Aksenov and Inna V Aksenova and Sergey G Krivokolysko},
title = {Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles},
journal = {Chemistry of Heterocyclic Compounds},
year = {2017},
volume = {53},
publisher = {Springer Nature},
month = {aug},
url = {https://doi.org/10.1007/s10593-017-2140-7},
number = {8},
pages = {887--891},
doi = {10.1007/s10593-017-2140-7}
}
Cite this
MLA
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Khrustaleva, Anastasiya N., et al. “Aminomethylation of Guareschi imides: synthesis of 2,4-dioxo-1H,5H-3,7-spiro[diazabicyclo[3.3.1]nonane-9,4'-piperidine]-1,5-dicarbonitriles.” Chemistry of Heterocyclic Compounds, vol. 53, no. 8, Aug. 2017, pp. 887-891. https://doi.org/10.1007/s10593-017-2140-7.