Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene
Publication type: Journal Article
Publication date: 2019-12-23
scimago Q4
wos Q4
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Abstract
2,4,6-Trihydroxytoluene (2-methylphloroglucinol) was used as starting material for the first synthesis of several (Z)-2-arylidene-4,6-dihydroxy-7-methylaurones, including a synthetic analog of the natural 7-methylaureusidin, which is currently obtained mainly from the extract of sedge capitata (Cyperus capitatus). It was shown that the reaction of 2,4,6-trihydroxytoluene with chloroacetonitrile occurred regioselectively, with the formation of 4,6-dihydroxy-7-methylbenzofuran-3(2H)-one, the treatment of which with substituted benzaldehydes gave high yields of the target compounds.
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Shubin D. A. et al. Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene // Chemistry of Heterocyclic Compounds. 2019. Vol. 55. No. 12. pp. 1174-1178.
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Shubin D. A., Kuznetsov D. N., Kobrakov K. I., Starosotnikov A. M., Merkulova N. L. Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene // Chemistry of Heterocyclic Compounds. 2019. Vol. 55. No. 12. pp. 1174-1178.
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TY - JOUR
DO - 10.1007/s10593-019-02597-0
UR - https://doi.org/10.1007/s10593-019-02597-0
TI - Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene
T2 - Chemistry of Heterocyclic Compounds
AU - Shubin, Dmitry A
AU - Kuznetsov, Dmitry N
AU - Kobrakov, Konstantin I.
AU - Starosotnikov, Alexey M
AU - Merkulova, Natalya L
PY - 2019
DA - 2019/12/23
PB - Springer Nature
SP - 1174-1178
IS - 12
VL - 55
SN - 0009-3122
SN - 1573-8353
ER -
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@article{2019_Shubin,
author = {Dmitry A Shubin and Dmitry N Kuznetsov and Konstantin I. Kobrakov and Alexey M Starosotnikov and Natalya L Merkulova},
title = {Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene},
journal = {Chemistry of Heterocyclic Compounds},
year = {2019},
volume = {55},
publisher = {Springer Nature},
month = {dec},
url = {https://doi.org/10.1007/s10593-019-02597-0},
number = {12},
pages = {1174--1178},
doi = {10.1007/s10593-019-02597-0}
}
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MLA
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Shubin, Dmitry A., et al. “Synthesis of aurone derivatives on the basis of 2,4,6-trihydroxytoluene.” Chemistry of Heterocyclic Compounds, vol. 55, no. 12, Dec. 2019, pp. 1174-1178. https://doi.org/10.1007/s10593-019-02597-0.
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