β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles
Тип публикации: Journal Article
Дата публикации: 2019-12-26
scimago Q4
wos Q4
БС3
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Краткое описание
Novel water-soluble sulfonyl azides were synthesized, which are basic by nature. The obtained compounds were used as donors of the diazo group in the diazo transfer reaction. Due to their good solubility in water and high polarity, the byproducts formed in this case were easily separated from the desired products by washing with water or column chromatography. It was also shown that new sulfonyl azides as a result of reactions can be incorporated in heterocyclic products, imparting them water solubility.
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Shafran Y. M. et al. β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles // Chemistry of Heterocyclic Compounds. 2019. Vol. 55. No. 12. pp. 1251-1261.
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Shafran Y. M., Silaichev P. S., Bakulev V. A. β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles // Chemistry of Heterocyclic Compounds. 2019. Vol. 55. No. 12. pp. 1251-1261.
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TY - JOUR
DO - 10.1007/s10593-019-02609-z
UR - https://doi.org/10.1007/s10593-019-02609-z
TI - β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles
T2 - Chemistry of Heterocyclic Compounds
AU - Shafran, Yuri M
AU - Silaichev, Pavel S
AU - Bakulev, Vasiliy A
PY - 2019
DA - 2019/12/26
PB - Springer Nature
SP - 1251-1261
IS - 12
VL - 55
SN - 0009-3122
SN - 1573-8353
ER -
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@article{2019_Shafran,
author = {Yuri M Shafran and Pavel S Silaichev and Vasiliy A Bakulev},
title = {β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles},
journal = {Chemistry of Heterocyclic Compounds},
year = {2019},
volume = {55},
publisher = {Springer Nature},
month = {dec},
url = {https://doi.org/10.1007/s10593-019-02609-z},
number = {12},
pages = {1251--1261},
doi = {10.1007/s10593-019-02609-z}
}
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MLA
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Shafran, Yuri M., et al. “β-(Cycloalkylamino)ethanesulfonyl azides as novel water-soluble reagents for the synthesis of diazo compounds and heterocycles.” Chemistry of Heterocyclic Compounds, vol. 55, no. 12, Dec. 2019, pp. 1251-1261. https://doi.org/10.1007/s10593-019-02609-z.