Springer Nature
Chemistry of Heterocyclic Compounds
,  том 57 ,  издание 1 ,  страницы 20-25

Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation

Тип публикации: Journal Article
Дата публикации: 2021-01-01
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ISSN: 00093122, 15738353
Organic Chemistry
Краткое описание
Protonation of propargylsilanes induces 1,2-silyl group shift and provides 2-silylated dienes. If this reaction is performed in liquid SO2, the diene formation is followed by instant cheletropic SO2 addition, and 3-silylated 3-sulfolenes are obtained. Liquid SO2 as polar and Lewis acidic reaction medium makes it possible to use relatively weak Brønsted acid catalysts such as H2O and benzoic acid. Depending on the starting material, reductive desulfitation of 3-silylated 3-sulfolenes provides vinyl, allyl, or aliphatic silanes.
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Beļaunieks R. et al. Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation // Chemistry of Heterocyclic Compounds. 2021. Vol. 57. No. 1. pp. 20-25.
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Beļaunieks R., Puriņš M., Kumpins V., Turks M. Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation // Chemistry of Heterocyclic Compounds. 2021. Vol. 57. No. 1. pp. 20-25.
RIS |
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TY - JOUR
DO - 10.1007/s10593-021-02862-1
UR - https://doi.org/10.1007/s10593-021-02862-1
TI - Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation
T2 - Chemistry of Heterocyclic Compounds
AU - Beļaunieks, Rūdolfs
AU - Puriņš, Mikus
AU - Kumpins, Viktors
AU - Turks, Māris
PY - 2021
DA - 2021/01/01
PB - Springer Nature
SP - 20-25
IS - 1
VL - 57
SN - 0009-3122
SN - 1573-8353
ER -
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@article{2021_Beļaunieks,
author = {Rūdolfs Beļaunieks and Mikus Puriņš and Viktors Kumpins and Māris Turks},
title = {Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation},
journal = {Chemistry of Heterocyclic Compounds},
year = {2021},
volume = {57},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s10593-021-02862-1},
number = {1},
pages = {20--25},
doi = {10.1007/s10593-021-02862-1}
}
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Beļaunieks, Rūdolfs, et al. “Synthesis of 3-Silylated 3-Sulfolenes from Propargylsilanes and their Reductive Desulfitation.” Chemistry of Heterocyclic Compounds, vol. 57, no. 1, Jan. 2021, pp. 20-25. https://doi.org/10.1007/s10593-021-02862-1.
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