Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases
Publication type: Journal Article
Publication date: 2021-03-25
scimago Q4
wos Q4
SJR: 0.243
CiteScore: 2.7
Impact factor: 1.0
ISSN: 00093122, 15738353
Organic Chemistry
Abstract
Electrocatalytic transformation of aldehydes with two equivalents of 1,3-diethyl-2-thiobarbituric acid has been carried out in alcohols in an undivided cell in the presence of sodium halides with the selective formation of the substituted 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) in 87–98% yields and with 870–980% current efficiency. This new one-pot electrochemically induced tandem Knoevenagel–Michael process is a simple and efficient approach to substituted 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) containing two 1,3-diethyl-2-thiobarbituric acid fragments separated by C-aryl-substituted spacer, which are promising compounds for different biomedical applications, including anticonvulsant, antiAIDS agents and anti-inflammatory remedies. Theoretical studies were carried out to investigate the interaction of the synthesized compounds with beef and human catalases.
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Elinson M. N. et al. Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases // Chemistry of Heterocyclic Compounds. 2021. Vol. 57. No. 3. pp. 274-283.
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Elinson M. N., Vereshchagin A. N., Ryzhkova Y. E., Karpenko K. A., Ryzhkov F. V., Egorov M. P. Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases // Chemistry of Heterocyclic Compounds. 2021. Vol. 57. No. 3. pp. 274-283.
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TY - JOUR
DO - 10.1007/s10593-021-02904-8
UR - https://doi.org/10.1007/s10593-021-02904-8
TI - Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases
T2 - Chemistry of Heterocyclic Compounds
AU - Elinson, Michail N
AU - Vereshchagin, Anatoly N.
AU - Ryzhkova, Yuliya E
AU - Karpenko, Kirill A
AU - Ryzhkov, Fedor V
AU - Egorov, Mikhail P.
PY - 2021
DA - 2021/03/25
PB - Springer Nature
SP - 274-283
IS - 3
VL - 57
SN - 0009-3122
SN - 1573-8353
ER -
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@article{2021_Elinson,
author = {Michail N Elinson and Anatoly N. Vereshchagin and Yuliya E Ryzhkova and Kirill A Karpenko and Fedor V Ryzhkov and Mikhail P. Egorov},
title = {Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases},
journal = {Chemistry of Heterocyclic Compounds},
year = {2021},
volume = {57},
publisher = {Springer Nature},
month = {mar},
url = {https://doi.org/10.1007/s10593-021-02904-8},
number = {3},
pages = {274--283},
doi = {10.1007/s10593-021-02904-8}
}
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MLA
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Elinson, Michail N., et al. “Electrocatalytic tandem assembly of aldehydes with 2-thiobarbituric acid into 5,5'-(arylmethylene)bis(1,3-diethyl-2-thiobarbituric acids) and evaluation of their interaction with catalases.” Chemistry of Heterocyclic Compounds, vol. 57, no. 3, Mar. 2021, pp. 274-283. https://doi.org/10.1007/s10593-021-02904-8.