Journal of Cluster Science

, volume 25 , issue 4 , pages 937-947

Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate

MASOUD SALAVATI-NIASARI ^{1, 2}

Azam Sobhani ³

Sanaz Khoshrooz ¹

Noshin Mirzanasiri ⁴

Hide authors affiliations Show authors affiliations: 4 affiliations

Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, Islamic Republic of Iran |

Institute of Nano Science and Nano Technology, University of Kashan, Kashan, Islamic Republic of Iran |

Department of Chemistry, Kosar University of Bojnord, Bojnord, Islamic Republic of Iran |

⁴

School of Chemistry, College of Science, University of Tehran, Tehran, Islamic Republic of Iran |

Publication type: Journal Article

Publication date: 2013-12-04

Springer Nature

Journal of Cluster Science

scimago Q2

wos Q1

SJR: 0.515

CiteScore: 6.7

Impact factor: 3.6

ISSN: 10407278, 15728862

DOI: 10.1007/s10876-013-0674-0

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General Chemistry

Biochemistry

Condensed Matter Physics

General Materials Science

Abstract

PbS nanoparticles have been successfully synthesized through a simple, rapid microwave route using lead (II) oxalate as precursor, [Pb(O4C2)]. In this study, four different sulfur sources were applied that including sodium thiosulfate (Na2S2O3), thioacetamide (NH2CSCH3), thioglycolic acid (HSCH2CO2H), and l-cysteine (HO2CCH(NH2)CH2SH). The effects of sulfur sources on morphology and size of products in two different solvents, ethylene glycol (EG) and poly EG (PEG 400), were investigated. The products were analyzed by X-ray diffraction analysis, scanning electron microscopy, Fourier transform infrared spectroscopy and X-ray energy dispersive spectroscopy. Photoluminescence was used to study the optical properties of PbS nanoparticles.

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SALAVATI-NIASARI M. et al. Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate // Journal of Cluster Science. 2013. Vol. 25. No. 4. pp. 937-947.

GOST all authors (up to 50) Copy

SALAVATI-NIASARI M., Sobhani A., Khoshrooz S., Mirzanasiri N. Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate // Journal of Cluster Science. 2013. Vol. 25. No. 4. pp. 937-947.

RIS |

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RIS Copy

TY - JOUR

DO - 10.1007/s10876-013-0674-0

UR - https://doi.org/10.1007/s10876-013-0674-0

TI - Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate

T2 - Journal of Cluster Science

AU - SALAVATI-NIASARI, MASOUD

AU - Sobhani, Azam

AU - Khoshrooz, Sanaz

AU - Mirzanasiri, Noshin

PY - 2013

DA - 2013/12/04

PB - Springer Nature

SP - 937-947

IS - 4

VL - 25

SN - 1040-7278

SN - 1572-8862

ER -

BibTex |

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BibTex (up to 50 authors) Copy

@article{2013_SALAVATI-NIASARI,

author = {MASOUD SALAVATI-NIASARI and Azam Sobhani and Sanaz Khoshrooz and Noshin Mirzanasiri},

title = {Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate},

journal = {Journal of Cluster Science},

year = {2013},

volume = {25},

publisher = {Springer Nature},

month = {dec},

url = {https://doi.org/10.1007/s10876-013-0674-0},

number = {4},

pages = {937--947},

doi = {10.1007/s10876-013-0674-0}

}

MLA

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MLA Copy

SALAVATI-NIASARI, MASOUD, et al. “Preparation and Characterization of PbS Nanoparticles via Cyclic Microwave Radiation Using Precursor of Lead (II) Oxalate.” Journal of Cluster Science, vol. 25, no. 4, Dec. 2013, pp. 937-947. https://doi.org/10.1007/s10876-013-0674-0.

Publisher

Springer Nature

Journal

Journal of Cluster Science

scimago Q2

wos Q1

SJR

0.515

CiteScore

6.7

Impact factor

3.6

ISSN

10407278 (Print)

15728862 (Electronic)