Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials
Тип публикации: Journal Article
Дата публикации: 2016-04-13
SCImago Q2
WOS Q1
БС1
SJR: 0.6
CiteScore: 5.6
Impact factor: 4.2
ISSN: 09280707, 15734846
Materials Chemistry
General Chemistry
Ceramics and Composites
Electronic, Optical and Magnetic Materials
Condensed Matter Physics
Biomaterials
Краткое описание
Silica- or meso-silica- or silica-meso-silica-coated copper oxide microspheres were prepared based on base hydrolysis of tetraethyl orthosilicate in the presence of CuO and CTAB. Functionalization with amine or thiol organofunctional groups was conducted onto the surface of silica-meso-silica-coated copper oxide microspheres (Scheme 1). The silica-coated CuO composites and their amine- or thiol-functionalized materials have been characterized by TEM, XRD, TGA, FTIR and UV/Vis. TEM analysis showed that the CuO nanoparticles were encapsulated and dispersed into the silica or meso-silica microspheres. XRD analysis indicated that the size of CuO nanoparticles has decreased after coating with silica precursors. TGA and FTIR results indicated that the meso-silica-coated copper oxide materials have been successfully grafted by amine and thiol organofunctional groups.
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El-Nahhal I. M. et al. Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials // Journal of Sol-Gel Science and Technology. 2016. Vol. 79. No. 3. pp. 573-583.
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El-Nahhal I. M., SALEM J. K., Kuhn S., Hammad T., Hempelmann R., Al Bhaisi S. Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials // Journal of Sol-Gel Science and Technology. 2016. Vol. 79. No. 3. pp. 573-583.
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TY - JOUR
DO - 10.1007/s10971-016-4034-z
UR - https://doi.org/10.1007/s10971-016-4034-z
TI - Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials
T2 - Journal of Sol-Gel Science and Technology
AU - El-Nahhal, Issa M
AU - SALEM, JAMIL K.
AU - Kuhn, Sylvia
AU - Hammad, Talaat
AU - Hempelmann, Rolf
AU - Al Bhaisi, Sara
PY - 2016
DA - 2016/04/13
PB - Springer Nature
SP - 573-583
IS - 3
VL - 79
SN - 0928-0707
SN - 1573-4846
ER -
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@article{2016_El-Nahhal,
author = {Issa M El-Nahhal and JAMIL K. SALEM and Sylvia Kuhn and Talaat Hammad and Rolf Hempelmann and Sara Al Bhaisi},
title = {Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials},
journal = {Journal of Sol-Gel Science and Technology},
year = {2016},
volume = {79},
publisher = {Springer Nature},
month = {apr},
url = {https://doi.org/10.1007/s10971-016-4034-z},
number = {3},
pages = {573--583},
doi = {10.1007/s10971-016-4034-z}
}
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MLA
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El-Nahhal, Issa M., et al. “Synthesis and characterization of silica-, meso-silica- and their functionalized silica-coated copper oxide nanomaterials.” Journal of Sol-Gel Science and Technology, vol. 79, no. 3, Apr. 2016, pp. 573-583. https://doi.org/10.1007/s10971-016-4034-z.
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