Re-investigations of thermal decomposition of gadolinium sulfate octahydrate
Тип публикации: Journal Article
Дата публикации: 2010-02-18
SCImago Q2
WOS Q1
БС1
SJR: 0.554
CiteScore: 6.2
Impact factor: 4.1
ISSN: 13886150, 15882926, 03684466, 15728943, 14182874
Physical and Theoretical Chemistry
Condensed Matter Physics
Краткое описание
The crystals of Gd2(SO4)3·8H2O were obtained by slow crystallization from a saturated solution previously received by dissolving Gd2O3 in an aqueous solution of sulfuric acid. The thermal behavior of this salt was studied using simultaneous DTA–TG technique under a nitrogen and air, in the temperature range of 298–1773 K. It was found that the dehydration of gadolinium sulfate octahydrate as well as thermal decomposition of anhydrous Gd2(SO4)3 undergo in two steps. The existence of two polymorphic modification of anhydrous gadolinium sulfate has been confirmed. The new XRD data for high-temperature polymorph of Gd2(SO4)3 were given. All intermediate products of dehydration and thermal decomposition were characterized by EPR method.
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Tomaszewicz E., Leniec G., Kaczmarek S. M. Re-investigations of thermal decomposition of gadolinium sulfate octahydrate // Journal of Thermal Analysis and Calorimetry. 2010. Vol. 102. No. 3. pp. 875-881.
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Tomaszewicz E., Leniec G., Kaczmarek S. M. Re-investigations of thermal decomposition of gadolinium sulfate octahydrate // Journal of Thermal Analysis and Calorimetry. 2010. Vol. 102. No. 3. pp. 875-881.
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TY - JOUR
DO - 10.1007/s10973-010-0702-3
UR - https://doi.org/10.1007/s10973-010-0702-3
TI - Re-investigations of thermal decomposition of gadolinium sulfate octahydrate
T2 - Journal of Thermal Analysis and Calorimetry
AU - Tomaszewicz, E.
AU - Leniec, G
AU - Kaczmarek, S M
PY - 2010
DA - 2010/02/18
PB - Springer Nature
SP - 875-881
IS - 3
VL - 102
SN - 1388-6150
SN - 1588-2926
SN - 0368-4466
SN - 1572-8943
SN - 1418-2874
ER -
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@article{2010_Tomaszewicz,
author = {E. Tomaszewicz and G Leniec and S M Kaczmarek},
title = {Re-investigations of thermal decomposition of gadolinium sulfate octahydrate},
journal = {Journal of Thermal Analysis and Calorimetry},
year = {2010},
volume = {102},
publisher = {Springer Nature},
month = {feb},
url = {https://doi.org/10.1007/s10973-010-0702-3},
number = {3},
pages = {875--881},
doi = {10.1007/s10973-010-0702-3}
}
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Tomaszewicz, E., et al. “Re-investigations of thermal decomposition of gadolinium sulfate octahydrate.” Journal of Thermal Analysis and Calorimetry, vol. 102, no. 3, Feb. 2010, pp. 875-881. https://doi.org/10.1007/s10973-010-0702-3.
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