Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O
Тип публикации: Journal Article
Дата публикации: 2016-12-28
scimago Q2
wos Q2
БС1
SJR: 0.551
CiteScore: 7.7
Impact factor: 3.1
ISSN: 13886150, 15882926, 03684466, 15728943, 14182874
Physical and Theoretical Chemistry
Condensed Matter Physics
Краткое описание
The hexahydrate of europium nitrate hexahydrate Eu(NO3)3·6H2O shows no phase transitions in the range of −40 to 76 °C when it melts in its own water of crystallization. It was shown that the thermal decomposition is a complex step-wise process, which starts with the simultaneous condensation of 6 mol of the initial monomer Eu(NO3)3·6H2O into a cyclic cluster 6[Eu(NO3)3·6H2O]. This hexamer gradually loses water and nitric acid, and a series of intermediate amorphous oxynitrates is formed. The removal of HNO3 azeotrope is essentially a continuous process occurring in the liquid phase. At higher temperatures, oxynitrates undergo further degradation, lose water, nitrogen dioxide, and oxygen, and finally, after having lost lattice water, are transformed into europium oxide. All mass losses are satisfactorily accounted for under the proposed scheme of thermal decomposition.
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Melnikov P. et al. Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O // Journal of Thermal Analysis and Calorimetry. 2016. Vol. 128. No. 3. pp. 1353-1358.
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Melnikov P., Arkhangelsky I. V., Nascimento V. A., de OLIVEIRA L. C. S., Silva A. F., Zanoni L. Z. Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O // Journal of Thermal Analysis and Calorimetry. 2016. Vol. 128. No. 3. pp. 1353-1358.
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TY - JOUR
DO - 10.1007/s10973-016-6047-9
UR - https://doi.org/10.1007/s10973-016-6047-9
TI - Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O
T2 - Journal of Thermal Analysis and Calorimetry
AU - Melnikov, P
AU - Arkhangelsky, I V
AU - Nascimento, V A
AU - de OLIVEIRA, L. C. S.
AU - Silva, A. F.
AU - Zanoni, L Z
PY - 2016
DA - 2016/12/28
PB - Springer Nature
SP - 1353-1358
IS - 3
VL - 128
SN - 1388-6150
SN - 1588-2926
SN - 0368-4466
SN - 1572-8943
SN - 1418-2874
ER -
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@article{2016_Melnikov,
author = {P Melnikov and I V Arkhangelsky and V A Nascimento and L. C. S. de OLIVEIRA and A. F. Silva and L Z Zanoni},
title = {Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O},
journal = {Journal of Thermal Analysis and Calorimetry},
year = {2016},
volume = {128},
publisher = {Springer Nature},
month = {dec},
url = {https://doi.org/10.1007/s10973-016-6047-9},
number = {3},
pages = {1353--1358},
doi = {10.1007/s10973-016-6047-9}
}
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MLA
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Melnikov, P., et al. “Thermal properties of europium nitrate hexahydrate Eu(NO3)3·6H2O.” Journal of Thermal Analysis and Calorimetry, vol. 128, no. 3, Dec. 2016, pp. 1353-1358. https://doi.org/10.1007/s10973-016-6047-9.