Thermophysical study of graphene nanoflakes by differential scanning calorimetry
Тип публикации: Journal Article
Дата публикации: 2019-11-16
scimago Q2
wos Q2
БС1
SJR: 0.551
CiteScore: 7.7
Impact factor: 3.1
ISSN: 13886150, 15882926, 03684466, 15728943, 14182874
Physical and Theoretical Chemistry
Condensed Matter Physics
Краткое описание
Combustion heats of graphene nanoflakes (GNFs) of different thicknesses produced by chemical vapor deposition method were measured for the first time by differential scanning calorimetry (DSC) in the temperature range of 303–1273 K. They were found to be lower than that of graphite and increase nonlinearly from 18.8 ± 1.1 to 30.5 ± 1.4 kJ g −1 with decrease in the specific surface area of GNFs from 1730 to 770 m 2 g −1 . The heat capacity of GNFs was calculated to be higher than that of graphite. The energy diagram for the heat of GNF combustion was proposed based on the literature data and results of DSC, Raman spectroscopy and transmission electron microscopy study. The obtained results expand the scarce thermodynamic data available for graphene-based materials.
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Arkhipova E. A. et al. Thermophysical study of graphene nanoflakes by differential scanning calorimetry // Journal of Thermal Analysis and Calorimetry. 2019. Vol. 140. No. 6. pp. 2641-2648.
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Arkhipova E. A., Strokova N. E., Tambovtseva Y. A., Ivanov A. S., Chernyak S. A., Maslakov K. I., Egorova T. B., Savilov S. V., Lunin V. V. Thermophysical study of graphene nanoflakes by differential scanning calorimetry // Journal of Thermal Analysis and Calorimetry. 2019. Vol. 140. No. 6. pp. 2641-2648.
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TY - JOUR
DO - 10.1007/s10973-019-09040-8
UR - https://doi.org/10.1007/s10973-019-09040-8
TI - Thermophysical study of graphene nanoflakes by differential scanning calorimetry
T2 - Journal of Thermal Analysis and Calorimetry
AU - Arkhipova, Ekaterina A.
AU - Strokova, Natalia E
AU - Tambovtseva, Yulia A.
AU - Ivanov, Anton S.
AU - Chernyak, Sergei A.
AU - Maslakov, Konstantin I
AU - Egorova, Tolganay B
AU - Savilov, Serguei V.
AU - Lunin, Valery V.
PY - 2019
DA - 2019/11/16
PB - Springer Nature
SP - 2641-2648
IS - 6
VL - 140
SN - 1388-6150
SN - 1588-2926
SN - 0368-4466
SN - 1572-8943
SN - 1418-2874
ER -
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@article{2019_Arkhipova,
author = {Ekaterina A. Arkhipova and Natalia E Strokova and Yulia A. Tambovtseva and Anton S. Ivanov and Sergei A. Chernyak and Konstantin I Maslakov and Tolganay B Egorova and Serguei V. Savilov and Valery V. Lunin},
title = {Thermophysical study of graphene nanoflakes by differential scanning calorimetry},
journal = {Journal of Thermal Analysis and Calorimetry},
year = {2019},
volume = {140},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s10973-019-09040-8},
number = {6},
pages = {2641--2648},
doi = {10.1007/s10973-019-09040-8}
}
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MLA
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Arkhipova, Ekaterina A., et al. “Thermophysical study of graphene nanoflakes by differential scanning calorimetry.” Journal of Thermal Analysis and Calorimetry, vol. 140, no. 6, Nov. 2019, pp. 2641-2648. https://doi.org/10.1007/s10973-019-09040-8.