Journal of Nanoparticle Research, volume 11, issue 4, pages 995-1003
Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique
Publication type: Journal Article
Publication date: 2008-11-29
Journal:
Journal of Nanoparticle Research
Quartile SCImago
Q2
Quartile WOS
Q3
Impact factor: 2.5
ISSN: 13880764, 1572896X
General Chemistry
Atomic and Molecular Physics, and Optics
Condensed Matter Physics
General Materials Science
Bioengineering
Modeling and Simulation
Abstract
TiN, NbN, and TaN nanocrystals have been selectively prepared through a simple, solvent-free, and convenient reaction under autogenic pressure at moderate temperature (RAPET) process at 350 °C for 12 h, reacting transition metal chlorides and sodium azide. The nanostructures obtained are characterized by powder X-ray diffraction (PXRD), transmission electron microscopy (TEM), and scanning electron microscopy (SEM). A reaction mechanism is suggested based on the experimental results. These rapid reactions produce nanocrystals of TiN, NbN, and TaN with average sizes of approximately 30, 28, and 27 nm, respectively (as calculated from X-ray line broadening). An octahedral inorganic fullerene was detected among the various structures of the TiN.
Top-30
Citations by journals
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1 publication, 5.56%
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Chemical Engineering Journal
1 publication, 5.56%
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Carbon
1 publication, 5.56%
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1 publication, 5.56%
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1 publication, 5.56%
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1 publication, 5.56%
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Korean Journal of Materials Research
1 publication, 5.56%
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Advanced Materials
1 publication, 5.56%
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Zeitschrift fur Naturforschung - Section A Journal of Physical Sciences
1 publication, 5.56%
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Russian Chemical Reviews
1 publication, 5.56%
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Citations by publishers
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8
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Elsevier
8 publications, 44.44%
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Royal Society of Chemistry (RSC)
2 publications, 11.11%
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World Scientific
1 publication, 5.56%
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Springer Nature
1 publication, 5.56%
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Pleiades Publishing
1 publication, 5.56%
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Materials Research Society of Korea
1 publication, 5.56%
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Wiley
1 publication, 5.56%
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Walter de Gruyter
1 publication, 5.56%
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Autonomous Non-profit Organization Editorial Board of the journal Uspekhi Khimii
1 publication, 5.56%
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- We do not take into account publications without a DOI.
- Statistics recalculated only for publications connected to researchers, organizations and labs registered on the platform.
- Statistics recalculated weekly.
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George P. P. et al. Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique // Journal of Nanoparticle Research. 2008. Vol. 11. No. 4. pp. 995-1003.
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George P. P., Gedanken A., Makhlouf S. B. D., Genish I., Marcianò A., Abu Mukh R. Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique // Journal of Nanoparticle Research. 2008. Vol. 11. No. 4. pp. 995-1003.
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TY - JOUR
DO - 10.1007/s11051-008-9550-5
UR - https://doi.org/10.1007/s11051-008-9550-5
TI - Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique
T2 - Journal of Nanoparticle Research
AU - George, P. P.
AU - Gedanken, A.
AU - Makhlouf, Shirly Ben David
AU - Genish, I.
AU - Marcianò, A
AU - Abu Mukh, Riam
PY - 2008
DA - 2008/11/29 00:00:00
PB - Springer Nature
SP - 995-1003
IS - 4
VL - 11
SN - 1388-0764
SN - 1572-896X
ER -
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@article{2008_George,
author = {P. P. George and A. Gedanken and Shirly Ben David Makhlouf and I. Genish and A Marcianò and Riam Abu Mukh},
title = {Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique},
journal = {Journal of Nanoparticle Research},
year = {2008},
volume = {11},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11051-008-9550-5},
number = {4},
pages = {995--1003},
doi = {10.1007/s11051-008-9550-5}
}
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George, P. P., et al. “Synthesis and characterization of titanium nitride, niobium nitride, and tantalum nitride nanocrystals via the RAPET (reaction under autogenic pressure at elevated temperature) technique.” Journal of Nanoparticle Research, vol. 11, no. 4, Nov. 2008, pp. 995-1003. https://doi.org/10.1007/s11051-008-9550-5.