Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride
Publication type: Journal Article
Publication date: 2014-11-15
scimago Q3
wos Q4
SJR: 0.363
CiteScore: 3.3
Impact factor: 1.7
ISSN: 18785190, 18785204
Catalysis
Physical and Theoretical Chemistry
Abstract
Reduction of a Pd(II) precursor in refluxing 2-propanol, ethanol, or methanol in the presence of dissolved NaOH afforded silica-supported Pd catalysts designated Pd/SiO2(Pr), Pd/SiO2(Et), and Pd/SiO2(Me), respectively. Pd/SiO2(Pr) consisted of metallic Pd particles (average particle size, 5.1 nm) dispersed in the porous structure of SiO2, whereas the Pd particles on Pd/SiO2(Et) and Pd/SiO2(Me) were larger. The catalytic activity of Pd/SiO2(Pr) in the dechlorination of 2,4,6-trichloroanisole in a solution of 2-propanol containing NaOH was greatly enhanced by the addition of methanol; the optimum rate occurred at 1 % v/v methanol. The activity of Pd/SiO2(Et) was also enhanced by methanol but to a lesser extent than that of Pd/SiO2(Pr). In contrast, Pd/SiO2(Me) exhibited no activity even in the presence of methanol.
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Total citations:
11
Citations from 2025:
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(27.27%)
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UKISU Y. Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride // Reaction Kinetics, Mechanisms and Catalysis. 2014. Vol. 114. No. 2. pp. 385-394.
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UKISU Y. Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride // Reaction Kinetics, Mechanisms and Catalysis. 2014. Vol. 114. No. 2. pp. 385-394.
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TY - JOUR
DO - 10.1007/s11144-014-0807-y
UR - https://doi.org/10.1007/s11144-014-0807-y
TI - Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride
T2 - Reaction Kinetics, Mechanisms and Catalysis
AU - UKISU, Yuji
PY - 2014
DA - 2014/11/15
PB - Springer Nature
SP - 385-394
IS - 2
VL - 114
SN - 1878-5190
SN - 1878-5204
ER -
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BibTex (up to 50 authors)
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@article{2014_UKISU,
author = {Yuji UKISU},
title = {Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride},
journal = {Reaction Kinetics, Mechanisms and Catalysis},
year = {2014},
volume = {114},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11144-014-0807-y},
number = {2},
pages = {385--394},
doi = {10.1007/s11144-014-0807-y}
}
Cite this
MLA
Copy
UKISU, Yuji. “Preparation of silica-supported Pd nanoparticle catalysts by an alcohol reduction method and evaluation of their catalytic properties in the dechlorination of an aromatic chloride.” Reaction Kinetics, Mechanisms and Catalysis, vol. 114, no. 2, Nov. 2014, pp. 385-394. https://doi.org/10.1007/s11144-014-0807-y.