Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity
A A Taganova
1, 2
,
E A Boychenko
1, 2
,
N V Kiselev
1, 3
,
B B Khaidarov
1
,
E A Kolesnikov
1
,
A G Yudin
1
,
M A Vikulova
3
,
N V Gorshkov
3
,
D.V. KUZNETSOV
1
,
I N Burmistrov
1, 2
Publication type: Journal Article
Publication date: 2021-03-01
scimago Q3
wos Q4
SJR: 0.244
CiteScore: 0.8
Impact factor: 0.3
ISSN: 10834877, 15739139
Materials Chemistry
Ceramics and Composites
Abstract
The article investigates the influence of the reduction modes of hollow nickel oxide microspheres synthesized by the pyrolysis of ultrasonic aerosols on the ratio of the oxide and metallic forms of nickel in their structure. The synthesis of microspheres from an aerosol of an aqueous solution of nickel nitrate was carried out; their composition and morphology were studied. The reduction of microspheres was carried out in a stream of hydrogen at different temperatures. The ratio of metallic nickel and oxide was determined by two different methods: according to the data of thermogravimetric analysis and by the Rietveld method based on the results of x-ray phase analysis. It is shown that the proportion of metallic nickel increases with an increase in the reduction temperature to approximately 375°C and then changes insignificantly. The fractional composition of microspheres was determined.
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Taganova A. A. et al. Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity // Refractories and Industrial Ceramics. 2021. Vol. 61. No. 6. pp. 715-719.
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Taganova A. A., Boychenko E. A., Kiselev N. V., Khaidarov B. B., Kolesnikov E. A., Yudin A. G., Vikulova M. A., Gorshkov N. V., KUZNETSOV D., Burmistrov I. N. Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity // Refractories and Industrial Ceramics. 2021. Vol. 61. No. 6. pp. 715-719.
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TY - JOUR
DO - 10.1007/s11148-021-00548-x
UR - https://link.springer.com/10.1007/s11148-021-00548-x
TI - Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity
T2 - Refractories and Industrial Ceramics
AU - Taganova, A A
AU - Boychenko, E A
AU - Kiselev, N V
AU - Khaidarov, B B
AU - Kolesnikov, E A
AU - Yudin, A G
AU - Vikulova, M A
AU - Gorshkov, N V
AU - KUZNETSOV, D.V.
AU - Burmistrov, I N
PY - 2021
DA - 2021/03/01
PB - Springer Nature
SP - 715-719
IS - 6
VL - 61
SN - 1083-4877
SN - 1573-9139
ER -
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BibTex (up to 50 authors)
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@article{2021_Taganova,
author = {A A Taganova and E A Boychenko and N V Kiselev and B B Khaidarov and E A Kolesnikov and A G Yudin and M A Vikulova and N V Gorshkov and D.V. KUZNETSOV and I N Burmistrov},
title = {Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity},
journal = {Refractories and Industrial Ceramics},
year = {2021},
volume = {61},
publisher = {Springer Nature},
month = {mar},
url = {https://link.springer.com/10.1007/s11148-021-00548-x},
number = {6},
pages = {715--719},
doi = {10.1007/s11148-021-00548-x}
}
Cite this
MLA
Copy
Taganova, A. A., et al. “Synthesis and Study of the Composition of Hollow Microspheres of NiO and NiO/Ni Composition for Thermoelectrochemical Energy Converters of Low-Potential Temperature Gradients of Thermal Units Into Electricity.” Refractories and Industrial Ceramics, vol. 61, no. 6, Mar. 2021, pp. 715-719. https://link.springer.com/10.1007/s11148-021-00548-x.