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Russian Chemical Bulletin
,  том 58 ,  издание 4 ,  страницы 838-843

Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs

Тип публикации: Journal Article
Дата публикации: 2009-04-01
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SJR: 0.272
CiteScore: 2.8
Impact factor: 1.7
ISSN: 10665285, 15739171
General Chemistry
Краткое описание
A reaction of 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one with MeONa in MeOH to furnish 2-chloro-3-hydroxycyclopent-2-en-1,4-dione has been studied. The latter under the action of CH2N2 has been converted to the corresponding enol ether. This methodology has been used for the synthesis of 4-chloro-5-methoxy-2-cinnamylidenecyclopent-4-en-1,3-diones and related compounds starting from the parent dichlorocyclopentenone.
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Gimalova F. A. et al. Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs // Russian Chemical Bulletin. 2009. Vol. 58. No. 4. pp. 838-843.
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Gimalova F. A., Egorov V., Ivanova N. A., Fatykhov A. A., Miftakhov M. S. Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs // Russian Chemical Bulletin. 2009. Vol. 58. No. 4. pp. 838-843.
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TY - JOUR
DO - 10.1007/s11172-009-0103-6
UR - https://doi.org/10.1007/s11172-009-0103-6
TI - Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs
T2 - Russian Chemical Bulletin
AU - Gimalova, F A
AU - Egorov, V.A.
AU - Ivanova, N. A.
AU - Fatykhov, A A
AU - Miftakhov, M S
PY - 2009
DA - 2009/04/01
PB - Springer Nature
SP - 838-843
IS - 4
VL - 58
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2009_Gimalova,
author = {F A Gimalova and V.A. Egorov and N. A. Ivanova and A A Fatykhov and M S Miftakhov},
title = {Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs},
journal = {Russian Chemical Bulletin},
year = {2009},
volume = {58},
publisher = {Springer Nature},
month = {apr},
url = {https://doi.org/10.1007/s11172-009-0103-6},
number = {4},
pages = {838--843},
doi = {10.1007/s11172-009-0103-6}
}
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Gimalova, F. A., et al. “Unusual removal of the ethylene ketal protection from 2,3-dichloro-4,4-ethylenedioxycyclopent-2-en-1-one under alkaline conditions. Simple synthesis of naturally occurring cyclopentenedione analogs.” Russian Chemical Bulletin, vol. 58, no. 4, Apr. 2009, pp. 838-843. https://doi.org/10.1007/s11172-009-0103-6.
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