Springer Nature
Russian Chemical Bulletin
,  volume 58 ,  issue 11 ,  pages 2283-2287

Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate

Publication type: Journal Article
Publication date: 2009-11-01
Springer Nature
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Hydrogenation of heptamethyl cycloheptatrieneheptacarboxylate in the presence of palladium/carbon affords a stereoisomer of heptamethyl cyclohepteneheptacarboxylate with the cis-position of five ester groups in a yield of 60%, as well as the corresponding cyclohepta-1,3-dienes as trans,trans- and trans,cis-isomers. The reaction with sodium borohydride results in the stereoselective formation of bicyclic compound 5 upon reduction of one double bond and intramolecular cyclization. X-ray diffraction analysis of the compounds formed is carried out.
Found 
Found 

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GOST Copy
Platonov D. N. et al. Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate // Russian Chemical Bulletin. 2009. Vol. 58. No. 11. pp. 2283-2287.
GOST all authors (up to 50) Copy
Platonov D. N., Okonnishnikova G. P., Salikov R. F., Tomilov Yu. V. Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate // Russian Chemical Bulletin. 2009. Vol. 58. No. 11. pp. 2283-2287.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1007/s11172-009-0319-5
UR - https://doi.org/10.1007/s11172-009-0319-5
TI - Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate
T2 - Russian Chemical Bulletin
AU - Platonov, D N
AU - Okonnishnikova, G P
AU - Salikov, R F
AU - Tomilov, Yu V
PY - 2009
DA - 2009/11/01
PB - Springer Nature
SP - 2283-2287
IS - 11
VL - 58
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2009_Platonov,
author = {D N Platonov and G P Okonnishnikova and R F Salikov and Yu V Tomilov},
title = {Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate},
journal = {Russian Chemical Bulletin},
year = {2009},
volume = {58},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11172-009-0319-5},
number = {11},
pages = {2283--2287},
doi = {10.1007/s11172-009-0319-5}
}
MLA
Cite this
MLA Copy
Platonov, D. N., et al. “Reduction of the double bonds in heptamethyl cycloheptatriene-1,2,3,4,5,6,7-heptacarboxylate.” Russian Chemical Bulletin, vol. 58, no. 11, Nov. 2009, pp. 2283-2287. https://doi.org/10.1007/s11172-009-0319-5.