Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives
Publication type: Journal Article
Publication date: 2011-11-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
A potassium carbonate promoted addition of 2-bromonitroalkanes to methylidenemalonic and methylidenecyanoacetic acid derivatives and N-benzylmaleimide leads to the functionalized nitrocyclopropanes. In the case of less active olefins, it is reasonable to use the phase-transfer catalyst Bu4NPF6 (10 mol.%), whereas in the case of N-benzylmaleimide, to carry out the process in the ionic liquid [bmim]BF4.
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Kryshtal G. V. et al. Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives // Russian Chemical Bulletin. 2011. Vol. 60. No. 11. pp. 2279-2285.
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Kryshtal G. V., Zhdankina G. M., Shashkov A., Zlotin S. G. Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives // Russian Chemical Bulletin. 2011. Vol. 60. No. 11. pp. 2279-2285.
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TY - JOUR
DO - 10.1007/s11172-011-0348-8
UR - https://doi.org/10.1007/s11172-011-0348-8
TI - Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives
T2 - Russian Chemical Bulletin
AU - Kryshtal, G V
AU - Zhdankina, G M
AU - Shashkov, A.S
AU - Zlotin, S. G.
PY - 2011
DA - 2011/11/01
PB - Springer Nature
SP - 2279-2285
IS - 11
VL - 60
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2011_Kryshtal,
author = {G V Kryshtal and G M Zhdankina and A.S Shashkov and S. G. Zlotin},
title = {Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives},
journal = {Russian Chemical Bulletin},
year = {2011},
volume = {60},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11172-011-0348-8},
number = {11},
pages = {2279--2285},
doi = {10.1007/s11172-011-0348-8}
}
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MLA
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Kryshtal, G. V., et al. “Synthesis of nitrocyclopropanedicarboxylic acid derivatives by addition of α-bromonitroalkanes to methylidene malonic, methylidene cyanoacetic or maleic acid derivatives.” Russian Chemical Bulletin, vol. 60, no. 11, Nov. 2011, pp. 2279-2285. https://doi.org/10.1007/s11172-011-0348-8.