volume 61 issue 1 pages 131-135

The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles)

V V Dotsenko 1, 2
S G Krivokolysko 1
V P Litvinov 3
1
 
“ChemEx“ Laboratory Vladimir Dal’ East-Ukrainian National University, Lugansk, Ukraine
2
 
Physico-chemical Department, State Enterprise “Luganskstandartmetrology”, Lugansk, Ukraine
Publication typeJournal Article
Publication date2012-01-01
scimago Q3
SJR0.305
CiteScore2.8
Impact factor
ISSN10665285, 15739171
General Chemistry
Abstract
N-Methylmorpholinium 4-aryl-3-cyano-6-oxo-1,4,5,6-tetrahydropyridine-2-thiolates readily undergo the Mannich reaction with p-phenylenediamines and excess formaldehyde in the absence of a catalyst to form 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles) in moderate yields (24–56%).
Found 
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Dotsenko V. V. et al. The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles) // Russian Chemical Bulletin. 2012. Vol. 61. No. 1. pp. 131-135.
GOST all authors (up to 50) Copy
Dotsenko V. V., Krivokolysko S. G., Litvinov V. P. The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles) // Russian Chemical Bulletin. 2012. Vol. 61. No. 1. pp. 131-135.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1007/s11172-012-0018-5
UR - https://doi.org/10.1007/s11172-012-0018-5
TI - The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles)
T2 - Russian Chemical Bulletin
AU - Dotsenko, V V
AU - Krivokolysko, S G
AU - Litvinov, V P
PY - 2012
DA - 2012/01/01
PB - Springer Nature
SP - 131-135
IS - 1
VL - 61
SN - 1066-5285
SN - 1573-9171
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2012_Dotsenko,
author = {V V Dotsenko and S G Krivokolysko and V P Litvinov},
title = {The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles)},
journal = {Russian Chemical Bulletin},
year = {2012},
volume = {61},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s11172-012-0018-5},
number = {1},
pages = {131--135},
doi = {10.1007/s11172-012-0018-5}
}
MLA
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MLA Copy
Dotsenko, V. V., et al. “The Mannich reaction in the synthesis of N,S-containing heterocycles 11. Synthesis of 3,3′-(1,4-phenylene)-bis(8-aryl-6-oxo-3,4,7,8-tetrahydro-2H,6H-pyrido[2,1-b][1,3,5]thiadiazine-9-carbonitriles).” Russian Chemical Bulletin, vol. 61, no. 1, Jan. 2012, pp. 131-135. https://doi.org/10.1007/s11172-012-0018-5.