The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides
1
“ChemEx” Laboratory Vladimir Dal’ East-Ukrainian National University, Lugansk, Ukraine
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2
Physico-chemical Department, State Enterprise “Luganskstandartmetrology”, Lugansk, Ukraine
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Тип публикации: Journal Article
Дата публикации: 2012-01-01
scimago Q3
БС2
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Краткое описание
Piperidinium 6-amino-5-cyano-3-N-(4-methylphenyl)carbamoyl-4-phenyl-1,4-dihydro-pyridine-2-thiolate upon the action of primary amines and excess formaldehyde undergoes aminomethylation to form 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides in 36–52% yields.
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Dotsenko V. V. et al. The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides // Russian Chemical Bulletin. 2012. Vol. 61. No. 1. pp. 136-140.
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Dotsenko V. V., Krivokolysko S. G., Litvinov V. P. The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides // Russian Chemical Bulletin. 2012. Vol. 61. No. 1. pp. 136-140.
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TY - JOUR
DO - 10.1007/s11172-012-0019-4
UR - https://doi.org/10.1007/s11172-012-0019-4
TI - The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides
T2 - Russian Chemical Bulletin
AU - Dotsenko, V V
AU - Krivokolysko, S G
AU - Litvinov, V P
PY - 2012
DA - 2012/01/01
PB - Springer Nature
SP - 136-140
IS - 1
VL - 61
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2012_Dotsenko,
author = {V V Dotsenko and S G Krivokolysko and V P Litvinov},
title = {The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides},
journal = {Russian Chemical Bulletin},
year = {2012},
volume = {61},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s11172-012-0019-4},
number = {1},
pages = {136--140},
doi = {10.1007/s11172-012-0019-4}
}
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MLA
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Dotsenko, V. V., et al. “The Mannich reaction in the synthesis of N,S-containing heterocycles 12. First example of aminomethylation involving 2-thioxonicotinamide derivative: synthesis of 3,5,7,11-tetraazatricyclo[7.3.1.02,7]tridec-2-ene-9-carboxamides.” Russian Chemical Bulletin, vol. 61, no. 1, Jan. 2012, pp. 136-140. https://doi.org/10.1007/s11172-012-0019-4.
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