Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion
A. S. Kubasov
1, 2
,
E Yu Matveev
1, 2
,
V M Retivov
3
,
S S Akimov
1
,
G A Razgonyaeva
1
,
I N Polyakova
1
,
N A Votinova
1, 2
,
K Yu Zhizhin
1, 2
,
N. T. Kuznetsov
1, 2
2
3
Research Institute of Chemical Reactants and Ultrapure Compounds (IREA), Moscow, Russian Federation
|
Publication type: Journal Article
Publication date: 2014-01-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
The reactions of the salt (Bu4N)[2-B10H9O2C4H8] (1) with ammonia and ethylenediamine in ethanol were studied. These reactions afford substituted closo-decaborates with nitrogencontaining groups linked to the cluster through a diethylene glycol spacer. Using this method, we synthesized derivatives of the closo-decaborate anion with the pendant groups -NH3 + and -NHCH2CH2NH2; the complexes [Ni(H2O)(en)(L)] (7) and [Ni(en)(L)]·0.5H2O (8), where L = [2-B10H9O(CH2)2O(CH2)2NH(CH2)2NH2]2−, were synthesized. The X-ray diffraction study showed that the coordination sphere of the Ni2+ ions in complexes 7 and 8 have the same composition (4 N + 2 O). However, the coordination environment differs in the nature of the oxygen atom. Thus the oxygen atom directly bonded to the boron cluster is involved in the coordination of the metal ion in compound 8, whereas a water molecule is involved in the coordination in compound 7.
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Kubasov A. S. et al. Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion // Russian Chemical Bulletin. 2014. Vol. 63. No. 1. pp. 187-193.
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Kubasov A. S., Matveev E. Yu., Retivov V. M., Akimov S. S., Razgonyaeva G. A., Polyakova I. N., Votinova N. A., Zhizhin K. Yu., Kuznetsov N. T. Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion // Russian Chemical Bulletin. 2014. Vol. 63. No. 1. pp. 187-193.
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RIS
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TY - JOUR
DO - 10.1007/s11172-014-0412-2
UR - https://doi.org/10.1007/s11172-014-0412-2
TI - Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion
T2 - Russian Chemical Bulletin
AU - Kubasov, A. S.
AU - Matveev, E Yu
AU - Retivov, V M
AU - Akimov, S S
AU - Razgonyaeva, G A
AU - Polyakova, I N
AU - Votinova, N A
AU - Zhizhin, K Yu
AU - Kuznetsov, N. T.
PY - 2014
DA - 2014/01/01
PB - Springer Nature
SP - 187-193
IS - 1
VL - 63
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2014_Kubasov,
author = {A. S. Kubasov and E Yu Matveev and V M Retivov and S S Akimov and G A Razgonyaeva and I N Polyakova and N A Votinova and K Yu Zhizhin and N. T. Kuznetsov},
title = {Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion},
journal = {Russian Chemical Bulletin},
year = {2014},
volume = {63},
publisher = {Springer Nature},
month = {jan},
url = {https://doi.org/10.1007/s11172-014-0412-2},
number = {1},
pages = {187--193},
doi = {10.1007/s11172-014-0412-2}
}
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MLA
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Kubasov, A. S., et al. “Nickel(II) complexes with nitrogen-containing derivatives of the closo-decaborate anion.” Russian Chemical Bulletin, vol. 63, no. 1, Jan. 2014, pp. 187-193. https://doi.org/10.1007/s11172-014-0412-2.