Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives
Publication type: Journal Article
Publication date: 2016-03-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
A reaction of 1-(4,4-diethoxybutyl)-3-phenylthiourea with resorcinol, 2-methylresorcinol, pyrogallol, and hydroquinone in chloroform in the presence of trifluoroacetic acid leads to 2-aryl-1-(N-phenylcarbamothioyl)pyrrolidines. 1-(4,4-Diethoxybutyl)-3-arylureas and 1-(4,4diethoxybutyl)-3-arylthioureas in the presence of an acid catalyst undergo intramolecular cyclization and dimerization with the formation of 1,1´-bis(N-arylcarbamo(thio)yl)-2,3´-bipyrrole derivatives.
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Smolobochkin A. V. et al. Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives // Russian Chemical Bulletin. 2016. Vol. 65. No. 3. pp. 731-734.
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Smolobochkin A. V., Gazizov A. S., Voronina Yu. K., Burilov A. R., Pudovik M. A. Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives // Russian Chemical Bulletin. 2016. Vol. 65. No. 3. pp. 731-734.
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TY - JOUR
DO - 10.1007/s11172-016-1364-5
UR - https://doi.org/10.1007/s11172-016-1364-5
TI - Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives
T2 - Russian Chemical Bulletin
AU - Smolobochkin, A V
AU - Gazizov, A S
AU - Voronina, Yu K
AU - Burilov, A R
AU - Pudovik, M A
PY - 2016
DA - 2016/03/01
PB - Springer Nature
SP - 731-734
IS - 3
VL - 65
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2016_Smolobochkin,
author = {A V Smolobochkin and A S Gazizov and Yu K Voronina and A R Burilov and M A Pudovik},
title = {Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives},
journal = {Russian Chemical Bulletin},
year = {2016},
volume = {65},
publisher = {Springer Nature},
month = {mar},
url = {https://doi.org/10.1007/s11172-016-1364-5},
number = {3},
pages = {731--734},
doi = {10.1007/s11172-016-1364-5}
}
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Smolobochkin, A. V., et al. “Cyclization of 1-(4,4-diethoxybutyl)-3-aryl(thio)ureas to 2-arylpyrrolidines and 2,3´-bipyrrole derivatives.” Russian Chemical Bulletin, vol. 65, no. 3, Mar. 2016, pp. 731-734. https://doi.org/10.1007/s11172-016-1364-5.
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