Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives
E A Chigorina
1
,
K A Frolov
2, 3
,
V V Dotsenko
3, 4, 5
,
A S Goloveshkin
6
,
I S Bushmarinov
6
,
S G Krivokolysko
2, 3
3
ChemEx Laboratory, Vladimir Dal´ Lugansk State University, Molodezhnyi, Ukraine
|
Publication type: Journal Article
Publication date: 2016-09-01
scimago Q3
SJR: 0.305
CiteScore: 2.8
Impact factor: —
ISSN: 10665285, 15739171
General Chemistry
Abstract
Aminomethylation of triethylammonium 4-aryl-3,5-dicyano-6-oxo-1,4,5,6-tetrahydropyridin-2-olates and their sulfur and selenium analogs, as well as the structure of formed products, were studied in details. The reaction is of general character and leads to the formation of 7-substituted 9-aryl-2,4-dioxo-, 9-aryl-4-oxo-2-thioxo-, 9-aryl-4-oxo-2-selenoxo-3,7-diazabicyclo[3.3.1]nonane derivatives or their salts. The structures of ethyl 9-(2-chlorophenyl)-5-cyano-7-(4-methylphenyl)-2-oxo-4-thioxo-3,7-diazabicyclo[3.3.1]nonane-1-carboxylate (as a complex with N-methylmorpholine) and triethylammonium salt of 7-benzyl-4-oxo-2-selenoxo-9-(2-thienyl)-3,7-diazabicyclo[3.3.1]nonane-1,5-dicarbonitrile were studied by X-ray crystallography.
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Chigorina E. A. et al. Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives // Russian Chemical Bulletin. 2016. Vol. 65. No. 9. pp. 2260-2269.
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Chigorina E. A., Frolov K. A., Dotsenko V. V., Goloveshkin A. S., Bushmarinov I. S., Krivokolysko S. G. Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives // Russian Chemical Bulletin. 2016. Vol. 65. No. 9. pp. 2260-2269.
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RIS
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TY - JOUR
DO - 10.1007/s11172-016-1576-8
UR - https://doi.org/10.1007/s11172-016-1576-8
TI - Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives
T2 - Russian Chemical Bulletin
AU - Chigorina, E A
AU - Frolov, K A
AU - Dotsenko, V V
AU - Goloveshkin, A S
AU - Bushmarinov, I S
AU - Krivokolysko, S G
PY - 2016
DA - 2016/09/01
PB - Springer Nature
SP - 2260-2269
IS - 9
VL - 65
SN - 1066-5285
SN - 1573-9171
ER -
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BibTex (up to 50 authors)
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@article{2016_Chigorina,
author = {E A Chigorina and K A Frolov and V V Dotsenko and A S Goloveshkin and I S Bushmarinov and S G Krivokolysko},
title = {Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives},
journal = {Russian Chemical Bulletin},
year = {2016},
volume = {65},
publisher = {Springer Nature},
month = {sep},
url = {https://doi.org/10.1007/s11172-016-1576-8},
number = {9},
pages = {2260--2269},
doi = {10.1007/s11172-016-1576-8}
}
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MLA
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Chigorina, E. A., et al. “Synthesis and structure of new 3,7-diazabicyclo[3.3.1]nonane derivatives.” Russian Chemical Bulletin, vol. 65, no. 9, Sep. 2016, pp. 2260-2269. https://doi.org/10.1007/s11172-016-1576-8.