Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties
Тип публикации: Journal Article
Дата публикации: 2019-11-01
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SJR: 0.305
CiteScore: 2.8
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ISSN: 10665285, 15739171
General Chemistry
Краткое описание
An approach to p-tert-butylthiacalix[4]arene derivatives functionalized with lactic acid fragments in three conformations (cone, partial cone, 1,3-alternate) was developed. The use of tetraglyme as a solvent and magnesium sulfate with p-toluenesulfonic acid as co-condensation catalysts made it possible to obtain the desired products without admixtures of oligolactic acid. The structure of the synthesized macrocycles was characterized by a complex of physico-chemical methods. The thermal properties of the synthesized lactic acid copolyesters were studied by simultaneous thermogravimetry and differential scanning calorimetry analysis. Significant effect of the p-tert-butylthiacalix[4]arene platform on the thermal stability of the obtained products was demonstrated. Nanoscale particles of the synthesized macrocycles with a low polydispersity index were obtained using nanoprecipitation from methanol or acetone into a buffer solution.
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Reactive and Functional Polymers
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Russian Journal of Organic Chemistry
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Vavilova A. A. et al. Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties // Russian Chemical Bulletin. 2019. Vol. 68. No. 11. pp. 2098-2104.
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Vavilova A. A., Gorbachuk V., Shurpik D. N., Padnya P. L., Gerasimov A. V., Mostovaya O. A., Stoikov I. I. Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties // Russian Chemical Bulletin. 2019. Vol. 68. No. 11. pp. 2098-2104.
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TY - JOUR
DO - 10.1007/s11172-019-2672-3
UR - https://doi.org/10.1007/s11172-019-2672-3
TI - Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties
T2 - Russian Chemical Bulletin
AU - Vavilova, A A
AU - Gorbachuk, V.V
AU - Shurpik, D N
AU - Padnya, P L
AU - Gerasimov, A. V.
AU - Mostovaya, O A
AU - Stoikov, I I
PY - 2019
DA - 2019/11/01
PB - Springer Nature
SP - 2098-2104
IS - 11
VL - 68
SN - 1066-5285
SN - 1573-9171
ER -
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@article{2019_Vavilova,
author = {A A Vavilova and V.V Gorbachuk and D N Shurpik and P L Padnya and A. V. Gerasimov and O A Mostovaya and I I Stoikov},
title = {Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties},
journal = {Russian Chemical Bulletin},
year = {2019},
volume = {68},
publisher = {Springer Nature},
month = {nov},
url = {https://doi.org/10.1007/s11172-019-2672-3},
number = {11},
pages = {2098--2104},
doi = {10.1007/s11172-019-2672-3}
}
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Vavilova, A. A., et al. “Lactic acid copolyesters with carboxyl derivatives of p-tert-butylthiacalix[4]arene: synthesis and effect of macrocycle conformation on the physicochemical properties.” Russian Chemical Bulletin, vol. 68, no. 11, Nov. 2019, pp. 2098-2104. https://doi.org/10.1007/s11172-019-2672-3.