,
volume 31
,
issue 10
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pages 725-731
Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3 (Bipy)]
Publication type: Journal Article
Publication date: 2005-10-19
scimago Q4
wos Q4
SJR: 0.189
CiteScore: 1.7
Impact factor: 1.1
ISSN: 10703284, 16083318
General Chemistry
General Chemical Engineering
Abstract
The synthesis and X-ray diffraction analysis of [Gd[Thd)3(Bipy)] (HThd is dipivaloyl, and Bipy is 2,2′-bipyridyl) are performed. The crystals are triclinic, a = 11.095(5) Å, b = 12.263(3) Å, c = 18.357(4) Å, α = 79.43(2)°, β = 85.24(3)°, γ = 68.79(3)°, V = 2288.5(13) Å3, Z = 2, space group P1¯, and R = 0.0364 against 9125 reflections with I > 2σ(I). The Gd atom is bonded with six oxygen atoms of three dipivaloylmethanate ligands (with average Gd-O distance 2.343(3) Å) and two nitrogen atoms of the bipyridyl molecule (with average Gd-N distance 2.618(4) Å) at vertices of a distorted square antiprism. The stacking interaction is observed between the bipyridyl molecules linked by the inversion center of the complexes (the distance between the parallel Bipy planes is 3.45 Å).
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Minacheva L. Kh. et al. Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3(Bipy)] // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2005. Vol. 31. No. 10. pp. 725-731.
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Minacheva L. Kh., Rogachev A. Y., Sergienko V. S., Kuzmina N. P. Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3(Bipy)] // Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya. 2005. Vol. 31. No. 10. pp. 725-731.
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TY - JOUR
DO - 10.1007/s11173-005-0160-9
UR - https://doi.org/10.1007/s11173-005-0160-9
TI - Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3(Bipy)]
T2 - Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya
AU - Minacheva, L Kh
AU - Rogachev, A. Yu.
AU - Sergienko, V S
AU - Kuzmina, N. P.
PY - 2005
DA - 2005/10/19
PB - Pleiades Publishing
SP - 725-731
IS - 10
VL - 31
SN - 1070-3284
SN - 1608-3318
ER -
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@article{2005_Minacheva,
author = {L Kh Minacheva and A. Yu. Rogachev and V S Sergienko and N. P. Kuzmina},
title = {Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3(Bipy)]},
journal = {Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya},
year = {2005},
volume = {31},
publisher = {Pleiades Publishing},
month = {oct},
url = {https://doi.org/10.1007/s11173-005-0160-9},
number = {10},
pages = {725--731},
doi = {10.1007/s11173-005-0160-9}
}
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Minacheva, L. Kh., et al. “Synthesis and crystal structure of the heteroligand complex tris(dipivaloylmethanato)(2,2′-bipyridyl)gadolinium(III) [Gd(Thd) 3(Bipy)].” Russian Journal of Coordination Chemistry/Koordinatsionnaya Khimiya, vol. 31, no. 10, Oct. 2005, pp. 725-731. https://doi.org/10.1007/s11173-005-0160-9.
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