Pleiades Publishing
Russian Journal of Organic Chemistry
,  volume 40 ,  issue 12 ,  pages 1804-1809

1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals

Publication type: Journal Article
Publication date: 2004-12-01
Pleiades Publishing
scimago Q4
wos Q4
SJR: 0.190
CiteScore: 1.3
Impact factor: 0.9
ISSN: 10704280, 16083393
Organic Chemistry
Abstract
Reactions of trimethylsilyl azide with 3-trimethylsilyl-2-propynal and 2-propynal were studied. X-Ray analysis of the molecular structure of 4-trimethylsilyl-1H-1,2,3-triazole-5-carbaldehyde showed that the carbonyl group appears in the s-cis conformation with respect to the double C=C bond in the heteroring. The effect of the temperature and polarity of the medium on the ability of 1H-1,2,3-triazole-5-carbaldehyde to undergo dimerization to tricyclic bis-hemiaminals was examined by IR and 1H NMR spectroscopy.
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GOST Copy
Demina M. M. et al. 1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals // Russian Journal of Organic Chemistry. 2004. Vol. 40. No. 12. pp. 1804-1809.
GOST all authors (up to 50) Copy
Demina M. M., Novopashin P. S., Sarapulova G. I., Larina L. I., Smolin A. S., Fundamenskii V. S., Kashaev A. A., Medvedeva A. S. 1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals // Russian Journal of Organic Chemistry. 2004. Vol. 40. No. 12. pp. 1804-1809.
RIS |
Cite this
RIS Copy
TY - JOUR
DO - 10.1007/s11178-005-0103-4
UR - https://doi.org/10.1007/s11178-005-0103-4
TI - 1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals
T2 - Russian Journal of Organic Chemistry
AU - Demina, M M
AU - Novopashin, P S
AU - Sarapulova, G I
AU - Larina, L I
AU - Smolin, A S
AU - Fundamenskii, V S
AU - Kashaev, A. A.
AU - Medvedeva, A S
PY - 2004
DA - 2004/12/01
PB - Pleiades Publishing
SP - 1804-1809
IS - 12
VL - 40
SN - 1070-4280
SN - 1608-3393
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2004_Demina,
author = {M M Demina and P S Novopashin and G I Sarapulova and L I Larina and A S Smolin and V S Fundamenskii and A. A. Kashaev and A S Medvedeva},
title = {1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals},
journal = {Russian Journal of Organic Chemistry},
year = {2004},
volume = {40},
publisher = {Pleiades Publishing},
month = {dec},
url = {https://doi.org/10.1007/s11178-005-0103-4},
number = {12},
pages = {1804--1809},
doi = {10.1007/s11178-005-0103-4}
}
MLA
Cite this
MLA Copy
Demina, M. M., et al. “1,3-dipolar cycloaddition of trimethylsilyl azide to propynals and dimerization of 1H-1,2,3-triazole-5-carbaldehydes to tricyclic bis-hemiaminals.” Russian Journal of Organic Chemistry, vol. 40, no. 12, Dec. 2004, pp. 1804-1809. https://doi.org/10.1007/s11178-005-0103-4.