Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES)
Publication type: Journal Article
Publication date: 2022-06-01
scimago Q2
wos Q3
SJR: 0.431
CiteScore: 4.3
Impact factor: 2.5
ISSN: 03666352, 13369075, 25857290
Materials Chemistry
General Chemistry
Biochemistry
General Chemical Engineering
Industrial and Manufacturing Engineering
Abstract
Two methods for quantifying elemental impurities in a highly potent analgesic activity agent (2R,4aR,7R,8aR)-4,7-dimethyl-2-(thiophen-2-yl)octahydro-2H-chromen-4-ol have been developed using acid decomposition assisted by microwave digestion system or heating in metallic block followed by analyte determination using microwave-induced plasma optical emission spectrometry (MIP OES). Both methods have been validated. The fast linear interference correction (FLIC) and inter-element correction (IEC) methods have been used to take into account possible spectral interferences. Arsenic and mercury have been determined using the multimode sample introduction system (MSIS). The detection limits have been calculated (µg L−1) – 5.4 for Cd, 5.1 for Pb, 11 for As, 1.3 for Hg, 10 for Co, 2.4 for V, 1.4 for Ni. The accuracy of the results was established using an independent inductively coupled plasma mass spectrometry (ICP-MS) method. The relative standard deviation (RSD) (n ≥ 4) was ≤ 12% for Cd, 3.8% for Pb, 6.2% for As, 11% for Hg, 3.0% for V (sample decomposition assisted by heating on metallic block), and 10% for Ni (sample decomposition assisted by microwave radiation). It was shown that the concentration of Cd, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, and Mo as impurities in (2R,4aR,7R,8aR)-4,7-dimethyl-2-(thiophen-2-yl)octahydro-2H-chromen-4-ol was lower than the upper limit concentration.
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Zubricheva D. V. et al. Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES) // Chemical Papers. 2022. Vol. 76. No. 9. pp. 5677-5689.
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Zubricheva D. V., Lastovka A. V., Ilina I. V., Volcho K. P., Tikhova V. D., Fadeeva V. P., Salakhutdinov N. F. Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES) // Chemical Papers. 2022. Vol. 76. No. 9. pp. 5677-5689.
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TY - JOUR
DO - 10.1007/s11696-022-02275-0
UR - https://doi.org/10.1007/s11696-022-02275-0
TI - Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES)
T2 - Chemical Papers
AU - Zubricheva, Daria V
AU - Lastovka, Anastasiya V
AU - Ilina, Irina V
AU - Volcho, Konstantin P.
AU - Tikhova, Vera D
AU - Fadeeva, Valentina P
AU - Salakhutdinov, Nariman F.
PY - 2022
DA - 2022/06/01
PB - Springer Nature
SP - 5677-5689
IS - 9
VL - 76
SN - 0366-6352
SN - 1336-9075
SN - 2585-7290
ER -
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BibTex (up to 50 authors)
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@article{2022_Zubricheva,
author = {Daria V Zubricheva and Anastasiya V Lastovka and Irina V Ilina and Konstantin P. Volcho and Vera D Tikhova and Valentina P Fadeeva and Nariman F. Salakhutdinov},
title = {Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES)},
journal = {Chemical Papers},
year = {2022},
volume = {76},
publisher = {Springer Nature},
month = {jun},
url = {https://doi.org/10.1007/s11696-022-02275-0},
number = {9},
pages = {5677--5689},
doi = {10.1007/s11696-022-02275-0}
}
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MLA
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Zubricheva, Daria V., et al. “Determination of elemental impurities Cd, Pb, As, Hg, Co, V, Ni, Pd, Ru, Ag, Pt, Mo, Al, and Fe in highly potent analgesic activity agent by microwave-induced plasma optical emission spectrometry (MIP OES).” Chemical Papers, vol. 76, no. 9, Jun. 2022, pp. 5677-5689. https://doi.org/10.1007/s11696-022-02275-0.
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