Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography
1
Environmental Health Science Laboratory, Sumitomo Chemical Co. Ltd., 3-1-98, Kasugade-naka Konohana-ku, Osaka 554, Japan
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Тип публикации: Journal Article
Дата публикации: 1995-08-01
scimago Q1
wos Q1
БС1
SJR: 0.731
CiteScore: 7.3
Impact factor: 4.0
ISSN: 00219673, 18733778
Organic Chemistry
Biochemistry
General Medicine
Analytical Chemistry
Краткое описание
Enantiomeric separation of a thiazole derivative, (±)-(RS)-4-(2-fluoro-4-biphenylyl)ethyl]-2-methylaminothiazole can be achieved by HPLC using a β-cyclodextrin (CD)-bonded stationary phase. The effects of the type of CD, organic modifiers in the mobile phase and mobile phase pH on the retention and resolution were studied and optimum conditions were established. The enantiomers of the compound were also separated by micellar electrokinetic chromatography with β- or γ-CDs as chiral additives. The retention behaviour of some structurally related compounds was examined with the two techniques and the results were compared.
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Furuta R., Doi T. Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography // Journal of Chromatography A. 1995. Vol. 708. No. 2. pp. 245-251.
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Furuta R., Doi T. Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography // Journal of Chromatography A. 1995. Vol. 708. No. 2. pp. 245-251.
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TY - JOUR
DO - 10.1016/0021-9673(95)00403-A
UR - https://doi.org/10.1016/0021-9673(95)00403-A
TI - Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography
T2 - Journal of Chromatography A
AU - Furuta, Ritsuko
AU - Doi, Tadashi
PY - 1995
DA - 1995/08/01
PB - Elsevier
SP - 245-251
IS - 2
VL - 708
SN - 0021-9673
SN - 1873-3778
ER -
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@article{1995_Furuta,
author = {Ritsuko Furuta and Tadashi Doi},
title = {Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography},
journal = {Journal of Chromatography A},
year = {1995},
volume = {708},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/0021-9673(95)00403-A},
number = {2},
pages = {245--251},
doi = {10.1016/0021-9673(95)00403-A}
}
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Furuta, Ritsuko, and Tadashi Doi. “Enantiomeric separation of a thiazole derivative by high-performance liquid chromatography and micellar electrokinetic chromatography.” Journal of Chromatography A, vol. 708, no. 2, Aug. 1995, pp. 245-251. https://doi.org/10.1016/0021-9673(95)00403-A.