Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate
1
BioCIS-CNRS, Centre d'Etudes Pharmaceutiques, Rue J.B. Clément, F-92296 Châtenay-Malabry, France
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Publication type: Journal Article
Publication date: 1994-08-01
scimago Q3
wos Q3
SJR: 0.334
CiteScore: 3.2
Impact factor: 1.5
ISSN: 00404039, 18733581
Organic Chemistry
Drug Discovery
Biochemistry
Abstract
The chlorine atom in chlorodifluoromethyl epoxy ethers is unusually reactive towards butyllithium. This reactivity has been used to develop a concise synthesis of gem-difluoro2-ethoxy allylic alcohols from the commercially available ethylchlorodifluoroacetate. A concise synthesis of 3- gem -difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate in 3 steps has been developed.
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Bégué J., Bonnet-Delpon D., Rock M. H. Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate // Tetrahedron Letters. 1994. Vol. 35. No. 33. pp. 6097-6100.
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Bégué J., Bonnet-Delpon D., Rock M. H. Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate // Tetrahedron Letters. 1994. Vol. 35. No. 33. pp. 6097-6100.
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TY - JOUR
DO - 10.1016/0040-4039(94)88085-9
UR - https://doi.org/10.1016/0040-4039(94)88085-9
TI - Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate
T2 - Tetrahedron Letters
AU - Bégué, Jean-Pierre
AU - Bonnet-Delpon, Danièle
AU - Rock, Michael H.
PY - 1994
DA - 1994/08/01
PB - Elsevier
SP - 6097-6100
IS - 33
VL - 35
SN - 0040-4039
SN - 1873-3581
ER -
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@article{1994_Bégué,
author = {Jean-Pierre Bégué and Danièle Bonnet-Delpon and Michael H. Rock},
title = {Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate},
journal = {Tetrahedron Letters},
year = {1994},
volume = {35},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/0040-4039(94)88085-9},
number = {33},
pages = {6097--6100},
doi = {10.1016/0040-4039(94)88085-9}
}
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MLA
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Bégué, Jean-Pierre, et al. “Synthesis of 3-gem-difluoro-2-ethoxy allylic alcohols from ethyl chlorodifluoroacetate.” Tetrahedron Letters, vol. 35, no. 33, Aug. 1994, pp. 6097-6100. https://doi.org/10.1016/0040-4039(94)88085-9.