Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra
1
Celsius Materialteknik, S-691 51 Karlskoga, Sweden
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Publication type: Journal Article
Publication date: 1995-10-01
scimago Q2
wos Q1
SJR: 0.654
CiteScore: 7.4
Impact factor: 3.8
ISSN: 01697439, 18733239
Computer Science Applications
Spectroscopy
Analytical Chemistry
Process Chemistry and Technology
Software
Abstract
The main constituent in a propellant is nitrocellulose, which by nature is unstable, and consequently it has to be stabilised with, e.g., diphenylamine. In order to determine the remaining shelflife of the propellant, the amount of stabiliser is determined. The method mostly used for this purpose, high-performance liquid chromatography (HPLC), is however complex and time consuming. Partial least squares calibration of the infrared spectroscopic profiles of the stabiliser and its derivatives in the propellant against their respective quantities (determined by HPLC) was tested to find out whether the quantitative determination of the above was possible. The initial results show that the cross-validated calibration model yields quantitative determination of the stabiliser and its derivatives within an error limit of 10% in predicted values. The correlation between the measured and predicted values was better than 0.94 for the stabiliser and its three first derivatives.
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Lindblom T., Christy A. A., Libnau F. O. Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra // Chemometrics and Intelligent Laboratory Systems. 1995. Vol. 29. No. 2. pp. 243-254.
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Lindblom T., Christy A. A., Libnau F. O. Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra // Chemometrics and Intelligent Laboratory Systems. 1995. Vol. 29. No. 2. pp. 243-254.
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RIS
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TY - JOUR
DO - 10.1016/0169-7439(95)80099-U
UR - https://doi.org/10.1016/0169-7439(95)80099-U
TI - Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra
T2 - Chemometrics and Intelligent Laboratory Systems
AU - Lindblom, Torbjörn
AU - Christy, Alfred A
AU - Libnau, Fred O
PY - 1995
DA - 1995/10/01
PB - Elsevier
SP - 243-254
IS - 2
VL - 29
SN - 0169-7439
SN - 1873-3239
ER -
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BibTex (up to 50 authors)
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@article{1995_Lindblom,
author = {Torbjörn Lindblom and Alfred A Christy and Fred O Libnau},
title = {Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra},
journal = {Chemometrics and Intelligent Laboratory Systems},
year = {1995},
volume = {29},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/0169-7439(95)80099-U},
number = {2},
pages = {243--254},
doi = {10.1016/0169-7439(95)80099-U}
}
Cite this
MLA
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Lindblom, Torbjörn, et al. “Quantitative determination of stabiliser in a single base propellant by chemometric analysis of Fourier transform infrared spectra.” Chemometrics and Intelligent Laboratory Systems, vol. 29, no. 2, Oct. 1995, pp. 243-254. https://doi.org/10.1016/0169-7439(95)80099-U.