Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride
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Department of Chemistry, University of Joensuu, PO BOX 111, FIN-80101, Joensuu, Finland.
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Publication type: Journal Article
Publication date: 1998-04-01
scimago Q3
wos Q2
SJR: 0.385
CiteScore: 4.1
Impact factor: 2.4
ISSN: 0022328X, 18728561
Materials Chemistry
Organic Chemistry
Biochemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
The preparation and molecular structure of meso -(ethylenebis(2-(dimethylamino)indenyl))zirconium dichloride ( 3 ) is reported. Predominant meso formation is observed when the ligand dilithium salt is reacted with ZrCl 4 in THF. Complex 3 crystallizes in a chiral C 1 symmetric staggered conformation (Ind ∧ Ind=23.1°) and reveals shortened hapto–nitrogen bond lengths, 1.456(11) and 1.399(13) A, indicating extensive orbital overlap between the nitrogen and the hapto carbon atom.
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Luttikhedde H. J. et al. Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride // Journal of Organometallic Chemistry. 1998. Vol. 557. No. 2. pp. 227-230.
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Luttikhedde H. J., LEINO R., Ahlgrén M. J., Pakkanen T. A., Näsman J. H. Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride // Journal of Organometallic Chemistry. 1998. Vol. 557. No. 2. pp. 227-230.
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TY - JOUR
DO - 10.1016/S0022-328X(97)00694-3
UR - https://doi.org/10.1016/S0022-328X(97)00694-3
TI - Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride
T2 - Journal of Organometallic Chemistry
AU - Luttikhedde, Hendrik J.G.
AU - LEINO, R
AU - Ahlgrén, Markku J
AU - Pakkanen, Tapani A.
AU - Näsman, Jan H
PY - 1998
DA - 1998/04/01
PB - Elsevier
SP - 227-230
IS - 2
VL - 557
SN - 0022-328X
SN - 1872-8561
ER -
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BibTex (up to 50 authors)
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@article{1998_Luttikhedde,
author = {Hendrik J.G. Luttikhedde and R LEINO and Markku J Ahlgrén and Tapani A. Pakkanen and Jan H Näsman},
title = {Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride},
journal = {Journal of Organometallic Chemistry},
year = {1998},
volume = {557},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/S0022-328X(97)00694-3},
number = {2},
pages = {227--230},
doi = {10.1016/S0022-328X(97)00694-3}
}
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MLA
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Luttikhedde, Hendrik J.G., et al. “Synthesis and molecular structure of meso-(ethylenebis-(2-(dimethylamino)-1-indenyl))zirconium dichloride.” Journal of Organometallic Chemistry, vol. 557, no. 2, Apr. 1998, pp. 227-230. https://doi.org/10.1016/S0022-328X(97)00694-3.