Open Access

Catalysis Communications

, том 27 , страницы 184-188

Synthesis of glycidol from glycerol and dimethyl carbonate using ionic liquid as a catalyst

Swapna M Gade ¹

Mudassir K Munshi ¹

Batul M Chherawalla ¹

Vilas H Rane ¹

Ashutosh A. Kelkar ¹

Скрыть аффилиации авторов Показать аффилиации авторов: 1 аффилиация

Chemical Engineering and Process Development Division, National Chemical Laboratory, Pune-411008, India |

Тип публикации: Journal Article

Дата публикации: 2012-10-01

Elsevier

Catalysis Communications

scimago Q1

wos Q2

SJR: 0.811

CiteScore: 7.9

Impact factor: 4.3

ISSN: 15667367

DOI: 10.1016/j.catcom.2012.07.003

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General Chemistry

Catalysis

Process Chemistry and Technology

Краткое описание

Transesterification of dimethyl carbonate with glycerol has been investigated using various ionic liquids as catalysts. Synthesis of glycidol with high selectivity (78%) has been achieved using tetramethylammonium hydroxide ([TMA][OH]) as a catalyst at 80 °C. Effect of various reaction conditions on the activity and selectivity was investigated and catalyst concentration had a significant influence on conversion as well as selectivity to glycidol. Activity as well as selectivity of the catalyst decreased significantly with increase in moisture content. Recycle experiment indicated slight drop in glycerol conversion and selectivity to glycidol because of dilution of reaction mixture and also the presence of products from the initial experiment.

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Gade S. M. et al. Synthesis of glycidol from glycerol and dimethyl carbonate using ionic liquid as a catalyst // Catalysis Communications. 2012. Vol. 27. pp. 184-188.

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Gade S. M., Munshi M. K., Chherawalla B. M., Rane V. H., Kelkar A. A. Synthesis of glycidol from glycerol and dimethyl carbonate using ionic liquid as a catalyst // Catalysis Communications. 2012. Vol. 27. pp. 184-188.

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TY - JOUR

DO - 10.1016/j.catcom.2012.07.003

UR - https://doi.org/10.1016/j.catcom.2012.07.003

TI - Synthesis of glycidol from glycerol and dimethyl carbonate using ionic liquid as a catalyst

T2 - Catalysis Communications

AU - Gade, Swapna M

AU - Munshi, Mudassir K

AU - Chherawalla, Batul M

AU - Rane, Vilas H

AU - Kelkar, Ashutosh A.

PY - 2012

DA - 2012/10/01

PB - Elsevier

SP - 184-188

VL - 27

SN - 1566-7367

ER -

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@article{2012_Gade,

author = {Swapna M Gade and Mudassir K Munshi and Batul M Chherawalla and Vilas H Rane and Ashutosh A. Kelkar},

title = {Synthesis of glycidol from glycerol and dimethyl carbonate using ionic liquid as a catalyst},

journal = {Catalysis Communications},

year = {2012},

volume = {27},

publisher = {Elsevier},

month = {oct},

url = {https://doi.org/10.1016/j.catcom.2012.07.003},

pages = {184--188},

doi = {10.1016/j.catcom.2012.07.003}

}

Издатель

Elsevier

Журнал

Catalysis Communications

scimago Q1

wos Q2

SJR

0.811

CiteScore

7.9

Impact factor

4.3

ISSN

15667367 (Print)