Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection
1
Department of Pharmaceutical Chemistry, National Medicines Institute, 30/34 Chelmska Street, 00-725 Warsaw, Poland.
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2
Department of Pharmaceutical Chemistry, National Medicines Institute, 30/34 Chelmska Street, 00-725 Warsaw, Poland
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Тип публикации: Journal Article
Дата публикации: 2008-08-01
scimago Q1
wos Q1
БС1
SJR: 0.731
CiteScore: 7.3
Impact factor: 4.0
ISSN: 00219673, 18733778
PubMed ID:
18533165
Organic Chemistry
Biochemistry
General Medicine
Analytical Chemistry
Краткое описание
A sensitive and selective HPLC method with coulometric electrode array detection for the determination of pipecuronium bromide and its four impurities has been developed. The coulometric electrode array detection at increasing potentials from +300 to +900 mV of the porous graphite electrode versus the palladium reference electrode was used. The limit of detection and quantitation for pipecuronium bromide was 8 and 25 ng ml −1 , respectively. This elaborate method for the simultaneous analysis of pipecuronium bromide and its impurities proved to be fast, precise, accurate, sensitive, and could be applied to analysis in substances and in pharmaceutical preparations.
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Błażewicz A., Fijalek Z., Samsel K. Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection // Journal of Chromatography A. 2008. Vol. 1201. No. 2. pp. 191-195.
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Błażewicz A., Fijalek Z., Samsel K. Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection // Journal of Chromatography A. 2008. Vol. 1201. No. 2. pp. 191-195.
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TY - JOUR
DO - 10.1016/j.chroma.2008.05.008
UR - https://doi.org/10.1016/j.chroma.2008.05.008
TI - Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection
T2 - Journal of Chromatography A
AU - Błażewicz, Anna
AU - Fijalek, Zbigniew
AU - Samsel, Karolina
PY - 2008
DA - 2008/08/01
PB - Elsevier
SP - 191-195
IS - 2
VL - 1201
PMID - 18533165
SN - 0021-9673
SN - 1873-3778
ER -
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@article{2008_Błażewicz,
author = {Anna Błażewicz and Zbigniew Fijalek and Karolina Samsel},
title = {Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection},
journal = {Journal of Chromatography A},
year = {2008},
volume = {1201},
publisher = {Elsevier},
month = {aug},
url = {https://doi.org/10.1016/j.chroma.2008.05.008},
number = {2},
pages = {191--195},
doi = {10.1016/j.chroma.2008.05.008}
}
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Błażewicz, Anna, et al. “Determination of pipecuronium bromide and its impurities in pharmaceutical preparation by high-performance liquid chromatography with coulometric electrode array detection.” Journal of Chromatography A, vol. 1201, no. 2, Aug. 2008, pp. 191-195. https://doi.org/10.1016/j.chroma.2008.05.008.