Elsevier
Inorganic Chemistry Communication
,  volume 7 ,  issue 10 ,  pages 1135-1138

Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV)

Publication type: Journal Article
Publication date: 2004-10-01
Elsevier
scimago Q1
wos Q1
SJR: 0.758
CiteScore: 6.7
Impact factor: 5.4
ISSN: 13877003, 18790259
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Abstract
Bis{η5-(N,N-dimethylaminodimethylsilyl)tetramethylcyclopentadienyl}dichlorotitanium(IV), [TiCl2{η5-C5Me4(SiMe2NMe2)}2] (1), reacts with sulfane under cleavage of both Si–N and Ti–Cl bonds to give sulfido-tethered titanocene compound bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV), [Ti{η5-C5Me4(SiMe2S- κS)}2] (4), and dimethylamine hydrochloride as the byproduct. The crystal structure of compound 4 has been determined by single-crystal X-ray diffraction.
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Pinkas J. et al. Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV) // Inorganic Chemistry Communication. 2004. Vol. 7. No. 10. pp. 1135-1138.
GOST all authors (up to 50) Copy
Pinkas J., Gyepes R., Štěpnička P., Kubišta J., Horáček M., Mach K. Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV) // Inorganic Chemistry Communication. 2004. Vol. 7. No. 10. pp. 1135-1138.
RIS |
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RIS Copy
TY - JOUR
DO - 10.1016/j.inoche.2004.08.012
UR - https://doi.org/10.1016/j.inoche.2004.08.012
TI - Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV)
T2 - Inorganic Chemistry Communication
AU - Pinkas, J.
AU - Gyepes, Róbert
AU - Štěpnička, Petr
AU - Kubišta, Jiřı́
AU - Horáček, M.
AU - Mach, Karel
PY - 2004
DA - 2004/10/01
PB - Elsevier
SP - 1135-1138
IS - 10
VL - 7
SN - 1387-7003
SN - 1879-0259
ER -
BibTex |
Cite this
BibTex (up to 50 authors) Copy
@article{2004_Pinkas,
author = {J. Pinkas and Róbert Gyepes and Petr Štěpnička and Jiřı́ Kubišta and M. Horáček and Karel Mach},
title = {Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV)},
journal = {Inorganic Chemistry Communication},
year = {2004},
volume = {7},
publisher = {Elsevier},
month = {oct},
url = {https://doi.org/10.1016/j.inoche.2004.08.012},
number = {10},
pages = {1135--1138},
doi = {10.1016/j.inoche.2004.08.012}
}
MLA
Cite this
MLA Copy
Pinkas, J., et al. “Synthesis and structure of bis{η5-1,2,3,4-tetramethyl-5-(dimethylsilylsulfido-κS)cyclopentadienyl}titanium(IV).” Inorganic Chemistry Communication, vol. 7, no. 10, Oct. 2004, pp. 1135-1138. https://doi.org/10.1016/j.inoche.2004.08.012.