μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization
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Department of Chemistry, University of Louisiana at Lafayette, P.O. Box 44370 Lafayette, LA 70504, USA
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Тип публикации: Journal Article
Дата публикации: 2008-04-01
scimago Q1
wos Q1
БС2
SJR: 0.758
CiteScore: 6.7
Impact factor: 5.4
ISSN: 13877003, 18790259
Materials Chemistry
Inorganic Chemistry
Physical and Theoretical Chemistry
Краткое описание
A novel tricopper bridged oxalato complex with the structural formula [Cu(tacp)(H2O)]2[Cu(μ2-C2O4)2(ClO4)2] (1) where tacp = 1,4,8,12-tetraazacyclopentadecane was synthesized. The complex was characterized by X-ray crystallography and by spectroscopic techniques (IR and visible). The magnetic properties were also measured at variable temperatures (300–2 K). In this compound each oxalate is acting as a bridging ligand between two Cu2+ ions, where two types of coordination modes are found for the oxalate: monodentate and bidentate fashions. The magnetic coupling between the Cu–Cu centers is very weak antiferromagnetic (the singlet–triplet energy coupling J = −0.9 cm−1) and is in full agreement with the structural results.
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Louka F. R. et al. μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization // Inorganic Chemistry Communication. 2008. Vol. 11. No. 4. pp. 438-441.
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Louka F. R., Mautner F., Vicente R., Massoud S. μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization // Inorganic Chemistry Communication. 2008. Vol. 11. No. 4. pp. 438-441.
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TY - JOUR
DO - 10.1016/j.inoche.2008.01.019
UR - https://doi.org/10.1016/j.inoche.2008.01.019
TI - μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization
T2 - Inorganic Chemistry Communication
AU - Louka, Febee R
AU - Mautner, Franz-Andreas
AU - Vicente, Ramon
AU - Massoud, S.S.
PY - 2008
DA - 2008/04/01
PB - Elsevier
SP - 438-441
IS - 4
VL - 11
SN - 1387-7003
SN - 1879-0259
ER -
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@article{2008_Louka,
author = {Febee R Louka and Franz-Andreas Mautner and Ramon Vicente and S.S. Massoud},
title = {μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization},
journal = {Inorganic Chemistry Communication},
year = {2008},
volume = {11},
publisher = {Elsevier},
month = {apr},
url = {https://doi.org/10.1016/j.inoche.2008.01.019},
number = {4},
pages = {438--441},
doi = {10.1016/j.inoche.2008.01.019}
}
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Louka, Febee R., et al. “μ2-Oxalato-bridged tricopper(II) complex derived from 1,4,8,12-tetraazacyclopentadecane: Synthesis, structure and magnetic characterization.” Inorganic Chemistry Communication, vol. 11, no. 4, Apr. 2008, pp. 438-441. https://doi.org/10.1016/j.inoche.2008.01.019.