Synthesis, structure and properties of nanoparticles based on SrFe12-xRxO19 (R = Er, Tm) compounds
E.S. Vasilieva
1
,
Timur R. Nizamov
1
,
Maxim A. Abakumov
1, 2
,
Irina V. Dorofievich
1
,
Yulia A Baranova
1
,
Alexander D Kovalev
1
,
Polina I. Nikolenko
1
,
Bogdan D. Chernyshev
1
,
Ilya I. Rulev
1
,
Publication type: Journal Article
Publication date: 2023-11-01
scimago Q2
wos Q2
SJR: 0.521
CiteScore: 5.1
Impact factor: 3.0
ISSN: 03048853, 18734766
Electronic, Optical and Magnetic Materials
Condensed Matter Physics
Abstract
In this work a comprehensive analysis of the structure and properties of doped SrFe12-xRxO19 (R = Er, Tm) hexaferrites has been studied. The hexaferrtes were synthesized by two methods: mechanochemical and citrate approaches. The solubility of rare-earth elements (REE) has been studied by precision determination of the lattice spacings and cell volume of the samples, synthesized by mechanochemical method. It has been shown that the solubility of Er and Tm at a temperature of 1200 °C does not exceed × = 0.08 REE ions per formula unit. According to Mössbauer spectroscopy, REE atoms preferentially occupy 12 k positions. Nanoparticles of SrFe12-xRxO19 (R = Er, Tm) compounds for MRI were obtained by high-energy ball milling of the citrate samples for 50 h in an octadecene solution with oleic acid. Stable hydrosols of nanoparticles were obtained after their coating with Pluronic F127 polymer. It has been shown that the obtained nanoparticles can be used for biomedical applications as contrast agents.
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Vasilieva E. et al. Synthesis, structure and properties of nanoparticles based on SrFe12-xRxO19 (R = Er, Tm) compounds // Journal of Magnetism and Magnetic Materials. 2023. Vol. 585. p. 171127.
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Vasilieva E., Bordyuzhin I. G., Nizamov T. R., Nikitin A. A., Abakumov M. A., Dorofievich I. V., Baranova Y. A., Kovalev A. D., Nikolenko P. I., Chernyshev B. D., Rulev I. I., Shchetinin I. Synthesis, structure and properties of nanoparticles based on SrFe12-xRxO19 (R = Er, Tm) compounds // Journal of Magnetism and Magnetic Materials. 2023. Vol. 585. p. 171127.
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TY - JOUR
DO - 10.1016/j.jmmm.2023.171127
UR - https://doi.org/10.1016/j.jmmm.2023.171127
TI - Synthesis, structure and properties of nanoparticles based on SrFe12-xRxO19 (R = Er, Tm) compounds
T2 - Journal of Magnetism and Magnetic Materials
AU - Vasilieva, E.S.
AU - Bordyuzhin, Igor G.
AU - Nizamov, Timur R.
AU - Nikitin, Alexey A.
AU - Abakumov, Maxim A.
AU - Dorofievich, Irina V.
AU - Baranova, Yulia A
AU - Kovalev, Alexander D
AU - Nikolenko, Polina I.
AU - Chernyshev, Bogdan D.
AU - Rulev, Ilya I.
AU - Shchetinin, Igor
PY - 2023
DA - 2023/11/01
PB - Elsevier
SP - 171127
VL - 585
SN - 0304-8853
SN - 1873-4766
ER -
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BibTex (up to 50 authors)
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@article{2023_Vasilieva,
author = {E.S. Vasilieva and Igor G. Bordyuzhin and Timur R. Nizamov and Alexey A. Nikitin and Maxim A. Abakumov and Irina V. Dorofievich and Yulia A Baranova and Alexander D Kovalev and Polina I. Nikolenko and Bogdan D. Chernyshev and Ilya I. Rulev and Igor Shchetinin},
title = {Synthesis, structure and properties of nanoparticles based on SrFe12-xRxO19 (R = Er, Tm) compounds},
journal = {Journal of Magnetism and Magnetic Materials},
year = {2023},
volume = {585},
publisher = {Elsevier},
month = {nov},
url = {https://doi.org/10.1016/j.jmmm.2023.171127},
pages = {171127},
doi = {10.1016/j.jmmm.2023.171127}
}